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1,10-Phenanthroline hydrate

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1,10-Phenanthroline hydrate Basic information
1,10-Phenanthroline hydrate Chemical Properties
  • Melting point:100-104 °C(lit.)
  • Density 1.10
  • vapor density 6.2 (vs air)
  • storage temp. Sealed in dry,Room Temperature
  • solubility methanol: soluble200MM (Stock solution is stable for months at –20° C.)
  • form Needle-Like Crystals
  • color Off-white, may become cream-colored during storage
  • Water Solubility <0.01 g/100 mL at 21 ºC
  • Merck 14,7214
  • BRN 4008096
  • Stability:Stable. Incompatible with iron, other heavy metals, strong oxidizing agents, strong acids.
  • CAS DataBase Reference5144-89-8(CAS DataBase Reference)
  • EPA Substance Registry System1,10-Phenanthroline, monohydrate (5144-89-8)
Safety Information
  • Hazard Codes T,N
  • Risk Statements 25-50/53
  • Safety Statements 45-60-61
  • RIDADR UN 2811 6.1/PG 3
  • WGK Germany 3
  • RTECS SF8437000
  • TSCA Yes
  • HazardClass 6.1
  • PackingGroup III
  • HS Code 29339990
  • ToxicityLD50 orally in Rabbit: 132 mg/kg
MSDS
1,10-Phenanthroline hydrate Usage And Synthesis
  • Chemical Propertieswhite crystals or powder
  • UsesWhen complexed with copper, it possesses nuclease activity that has been used to study DNA-protein interactions.
  • General DescriptionWhite crystalline powder or solid. Slight odor.
  • Air & Water ReactionsInsoluble in water.
  • Reactivity Profile1,10-Phenanthroline hydrate is incompatible with strong oxidizers. 1,10-Phenanthroline hydrate is also incompatible with strong acids. 1,10-Phenanthroline hydrate forms complex compounds with ferrous ions. .
  • Fire HazardFlash point data for 1,10-Phenanthroline hydrate are not available. 1,10-Phenanthroline hydrate is probably combustible.
  • Purification MethodsCrystallise its picrate (m 191o) from EtOH; then the free base is liberated with aqueous alkali, dried at 78o/8mm over P2O5 and crystallised from pet ether (b 80-100o). [Cumper et al. J Chem Soc 1188 1962.] It can be purified by zone melting. It has also been crystallised from hexane, *benzene/pet ether (b 40-60o) or sodium-dried *benzene, dried and stored over H2SO4. The monohydrate is obtained by crystallisation from aqueous EtOH or ethyl acetate. It has been crystallised from H2O (300 parts) to give the monohydrate m 102-103o which sublimes at 10-3mm [Fielding & LeFevre J Chem Soc 1811 1951.] The anhydrous compound has m 118o (after drying at high vacuum at 80o) and is also obtained by recrystallisation from pet ether or *C6H6 (70 parts) and drying at 78o/8mm. [UV: Badger et al. J Chem Soc 3199 1951.] IthasapKainH2Oof 4.857 (25o) or 5.02 (20o) and 4.27 in 50% aqueous EtOH (20o). [Albert et al. J Chem Soc 2240 1948]. [Beilstein 23 H 227, 23 II 235, 23/8 V 419.]
1,10-Phenanthroline hydrate Preparation Products And Raw materials
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