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tert-Butyl chloroacetate

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tert-Butyl chloroacetate Basic information
tert-Butyl chloroacetate Chemical Properties
Safety Information
tert-Butyl chloroacetate Usage And Synthesis
  • Chemical Propertiesclear colorless to yellow liquid
  • UsesIn the glycidic ester condensation.
  • HazardA poison by ingestion. Moderately toxic by inhalation skin contact. Severe skin and moderate eye irritant.
  • Safety ProfileA poison by ingestion. Moderately toxic by inhalation skin contact. S severe sluin and moderate eye irritant. When heated to decomposition it emits toxic vapors of Cl-.
  • Purification MethodsCheck the NMR spectrum; if satisfactory then distil in a vacuum; if not then dissolve in Et2O, wash with H2O, 10% H2SO4 until the acid extract does not become cloudy when made alkaline with NaOH. Wash the organic layer again with H2O, then saturated aqueous NaHCO3, dry over Na2SO4, evaporate and fractionate it through a carborundum-packed column or a 6-inch Widmer column (p 11, see tert-butyl ethyl malonate for precautions to avoid decomposition during disillation). [Johnson et al. J Am Chem Soc 75 4995 1953, Baker Org Synth Coll Vol III 144 1944, Beilstein 2 III 444.]
tert-Butyl chloroacetate Preparation Products And Raw materials
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