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(R)-(+)-N,N-DIMETHYL-1-PHENYLETHYLAMINE

Basic information Safety Related Supplier
(R)-(+)-N,N-DIMETHYL-1-PHENYLETHYLAMINE Basic information
(R)-(+)-N,N-DIMETHYL-1-PHENYLETHYLAMINE Chemical Properties
  • Melting point:143°C (estimate)
  • Boiling point:81 °C16 mm Hg(lit.)
  • Density 0.908 g/mL at 25 °C(lit.)
  • FEMA 4248 | N,N-DIMETHYLPHENETHYLAMINE
  • refractive index n20/D 1.503(lit.)
  • Flash point:148 °F
  • storage temp. Refrigerator (+4°C)
  • pka8.88±0.50(Predicted)
  • optical activity[α]20/D +50.2°, c = 1 in methanol
  • JECFA Number1613
  • BRN 3030178
  • InChIKeyBVURNMLGDQYNAF-SECBINFHSA-N
  • CAS DataBase Reference19342-01-9(CAS DataBase Reference)
Safety Information
  • Hazard Codes Xi
  • Risk Statements 36/37/38
  • Safety Statements 26-36
  • WGK Germany 3
  • 8-10-23
  • HS Code 29214990
MSDS
(R)-(+)-N,N-DIMETHYL-1-PHENYLETHYLAMINE Usage And Synthesis
  • Chemical Propertiesclear colorless liquid
  • Chemical PropertiesColorless to yellow liquid; sweet fishy aroma.
  • Purification MethodsThe amine is mixed with aqueous 10N NaOH and extracted with toluene. The extract is washed with saturated aqueous NaCl, dried over K2CO3, and transferred to fresh K2CO3 until the solution is clear, and is filtered. The filtrate is distilled. If a short column packed with glass helices is used, the yield is reduced but a purer product is obtained. [Ingersoll Org Synth 25 89 1945, Snyder & Brewster J Am Chem Soc 71 291 4165 1949, Cope et al. J Am Chem Soc 71 3931 1949.] The (-)-picrate has m 140-141o from EtOH). The racemate [1126-71-2] has b 88-89o/16mm, 92-94o/30mm, 194-195o/760mm, d4 0.908. [Beilstein 13 III 2392.]
(R)-(+)-N,N-DIMETHYL-1-PHENYLETHYLAMINE(19342-01-9)Related Product Information
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