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(S)-(-)-N,N-DIMETHYL-1-PHENETHYLAMINE

Basic information Safety Related Supplier
(S)-(-)-N,N-DIMETHYL-1-PHENETHYLAMINE Basic information
(S)-(-)-N,N-DIMETHYL-1-PHENETHYLAMINE Chemical Properties
  • Melting point:143°C (estimate)
  • Boiling point:81 °C16 mm Hg(lit.)
  • Density 0.905 g/mL at 20 °C(lit.)
  • refractive index n20/D 1.503
  • Flash point:148 °F
  • storage temp.  0-6°C
  • pka8.88±0.50(Predicted)
  • optical activity[α]20/D 49.2°, c = 1 in methanol
  • BRN 3196218
  • CAS DataBase Reference17279-31-1(CAS DataBase Reference)
Safety Information
  • Hazard Codes Xn
  • Risk Statements 22-36
  • Safety Statements 26
  • RIDADR 2810
  • WGK Germany 2
  • 8-10-23
MSDS
(S)-(-)-N,N-DIMETHYL-1-PHENETHYLAMINE Usage And Synthesis
  • Chemical Propertiesclear colorless to yellow liquid
  • Purification MethodsThe amine is mixed with aqueous 10N NaOH and extracted with toluene. The extract is washed with saturated aqueous NaCl, dried over K2CO3, and transferred to fresh K2CO3 until the solution is clear, and is filtered. The filtrate is distilled. If a short column packed with glass helices is used, the yield is reduced but a purer product is obtained. [Ingersoll Org Synth 25 89 1945, Snyder & Brewster J Am Chem Soc 71 291 4165 1949, Cope et al. J Am Chem Soc 71 3931 1949.] The (-)-picrate has m 140-141o from EtOH). The racemate [1126-71-2] has b 88-89o/16mm, 92-94o/30mm, 194-195o/760mm, d4 0.908. [Beilstein 13 III 2392.]
(S)-(-)-N,N-DIMETHYL-1-PHENETHYLAMINE(17279-31-1)Related Product Information
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