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Acid Orange 7

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Acid Orange 7 Basic information
Acid Orange 7 Chemical Properties
  • Melting point:164°C
  • solubility Solubility Very soluble in water; very slightly soluble in ethanol
  • pka8.26, 11.4(at 25℃)
  • Colour Index 15510
  • form Crystalline Powder
  • color Green to blue
  • PH RangeAmber (7.4) to orange (8.6);Orange (10.2) to red (11.8)
  • Water Solubility 116 g/L (30 ºC)
  • λmax483nm
  • Merck 14,6858
  • BRN 3898201
  • Biological ApplicationsCosmetics; wound dressing materials
  • Major ApplicationOrganic light emitting diodes (OLEDs), nanoparticles, inks, wood preservatives, textiles, hair dyes, cosmetics, wound dressing materials, biofuel cells
  • CAS DataBase Reference633-96-5(CAS DataBase Reference)
  • EPA Substance Registry SystemBenzenesulfonic acid, 4-[(2-hydroxy-1-naphthalenyl) azo]-, monosodium salt(633-96-5)
Safety Information
  • Hazard Codes Xi
  • Risk Statements 36/37/38
  • Safety Statements 26-36-37/39
  • WGK Germany 3
  • RTECS DB7084000
  • HS Code 32041200
MSDS
Acid Orange 7 Usage And Synthesis
  • Chemical PropertiesOrange-red powder
  • Purification MethodsPurification is as for Orange I. Its solubility in H2O is 40g/L at 25o. [Müller et al. Helv Chim Acta 35 2579 1952.] Also purify it by extracting it with a small volume of cold water, then crystallising it by dissolving in boiling water, cooling to ca 80o, adding two volumes of EtOH and cooling. When cold, the precipitate is filtered off, washed with a little EtOH and dried in air. It can be salted out from aqueous solution with sodium acetate, then repeatedly extracted with EtOH. Meggy and Sims [J Chem Soc 2940 1956], after crystallising the sodium salt twice from water, dissolved it in cold water (11mL/g) and added conc HCl to precipitate the acid dye which was separated by centrifugation, redissolved and again precipitated with acid. After washing the precipitate three times with 0.5M acid, it was dried over NaOH, recrystallised twice from absolute EtOH, washed with a little Et2O, dried over NaOH and stored over conc H2SO4 in the dark. It can then be converted to the pure salt with the calculated amount of NaOH or Na2CO3. [Beilstein 16 IV 408.]
Acid Orange 7 Preparation Products And Raw materials
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