Chlorodiphenylphosphine
- Product Name:Chlorodiphenylphosphine
- CAS:1079-66-9
- MF:C12H10ClP
- MW:220.63
- EINECS:214-093-2
- Mol File:1079-66-9.mol
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Chlorodiphenylphosphine Chemical Properties
- Melting point:14-16°C
- Boiling point:320 °C(lit.)
- Density 1.229 g/mL at 25 °C(lit.)
- vapor density 7.8 (vs air)
- vapor pressure 1.3 hPa (20 °C)
- refractive index n
20/D 1.636(lit.)
- Flash point:>230 °F
- storage temp. Store below +30°C.
- solubility Miscible with alcohol. Slightly miscible with ammonia.
- form Liquid
- color Colorless to yellow
- Specific Gravity1.229
- Water Solubility Reacts violently
- Sensitive Air & Moisture Sensitive
- Hydrolytic Sensitivity8: reacts rapidly with moisture, water, protic solvents
- BRN 512032
- InChIKeyXGRJZXREYAXTGV-UHFFFAOYSA-N
- CAS DataBase Reference1079-66-9(CAS DataBase Reference)
- NIST Chemistry ReferenceChlorodiphenylphosphine(1079-66-9)
- EPA Substance Registry SystemPhosphinous chloride, diphenyl- (1079-66-9)
- Hazard Codes C
- Risk Statements 14-34-29-36
- Safety Statements 26-36/37/39-45-8-30-25-27
- RIDADR UN 3265 8/PG 2
- WGK Germany 2
- F 1-9-19
- Autoignition Temperature320 °C
- TSCA Yes
- HazardClass 8
- PackingGroup II
- HS Code 29310095
- ToxicityLD50 orally in Rabbit: 316 mg/kg
- Language:EnglishProvider:Chlorodiphenylphosphine
- Language:EnglishProvider:SigmaAldrich
- Language:EnglishProvider:ACROS
- Language:EnglishProvider:ALFA
Chlorodiphenylphosphine Usage And Synthesis
- Chemical PropertiesColorless to light yellow liqui
- Synthesis Reference(s)Journal of the American Chemical Society, 77, p. 3526, 1955 DOI: 10.1021/ja01618a030
- Purification MethodsThis air-sensitive, pale yellow lachrymatory liquid is purified by careful fractional distillation and discarding the lower boiling fraction which contains the main impurity PhPCl2 (b 48-51o/0.7mm), and checking for impurities by NMR. [Weinberg J Org Chem 40 3586 1975, Honer et al. Chem Ber 94 2122 1961, Beilstein 16 IV 969.]
Chlorodiphenylphosphine Preparation Products And Raw materials
- Preparation ProductsDiphenylphosphine1,1'-Bis(diphenylphosphino)ferroceneDimethylbisdiphenylphosphinoxanthene(R)-1-[(1S)-2-(DIPHENYLPHOSPHINO)FERROCENYL]ETHYLDI-TERT-BUTYLPHOSPHINE4-(DIMETHYLAMINO)PHENYLDIPHENYLPHOSPHINE(OXYDI-2,1-PHENYLENE)BIS(DIPHENYLPHOSPHINE)1-DIPHENYLPHOSPHINO-1'-(DI-TERT-BUTYLPH&
- BIS(4-METHOXYPHENYL)CHLOROPHOSPHINE Bis(triphenylphosphine)iminium chloride BIS(3,5-DIMETHYLPHENYL)CHLOROPHOSPHINE Chlorodiphenylphosphine sulfide BIS(3,5-DIMETHYL-4-METHOXYPHENYL)CHLOROPHOSPHINE BIS(3,5-DI(TRIFLUOROMETHYL)PHENYL)CHLOROPHOSPHINE DIPHENYLPHOSPHINYL CHLORIDE OR CHLORODIPHENYLPHOSPHINE OXIDE ORDIPHENYLPHOSPHINIC CHLORIDE,CHLORODIPHENYLPHOSPHINE OXIDE DI-O-TOLYLCHLOROPHOSPHINE Chlorodi(p-tolyl)phosphine, 95% DICHLOROTRIPHENYLPHOSPHORANE tert-Butylchlorodiphenylsilane Di-tert-butylchlorophosphane Diphenylsilanediol Methylene Chloride Tris(triphenylphosphine)rhodiu Tetrabutylphosphonium chloride Diphenylsilane Chlorodiphenylphosphine
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