Phenylphosphonic dichloride CAS#: 824-72-6

Phenylphosphonic dichloride

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Phenylphosphonic dichloride Basic information

Phenylphosphonic dichloride Chemical Properties

Melting point:3 °C(lit.)
Boiling point:258 °C(lit.)
Density 1.375 g/mL at 25 °C(lit.)
refractive index n20/D 1.559(lit.)
Flash point:>230 °F
storage temp. 2-8°C
solubility Miscible with benzene, chloroform, dimethyl sulfoxide and carbon tetrachloride.
form Liquid
color Clear yellow to brown
Specific Gravity1.394 (25℃)
Water Solubility reacts
λmax267nm(Cyclohexane)(lit.)
Sensitive Moisture Sensitive
BRN 1072240
InChIKeyIBDMRHDXAQZJAP-UHFFFAOYSA-N
CAS DataBase Reference824-72-6(CAS DataBase Reference)
NIST Chemistry ReferencePhosphonic dichloride, phenyl-(824-72-6)
EPA Substance Registry SystemPhosphonic dichloride, P-phenyl- (824-72-6)

Safety Information

MSDS

Phenylphosphonic dichloride Usage And Synthesis

Chemical PropertiesColorless to light yellow liqui
Synthesis Reference(s)Tetrahedron Letters, 33, p. 7473, 1992 DOI: 10.1016/S0040-4039(00)60798-0
Purification MethodsFractionally distil it using a very efficient or a spinning band column. [Lecher et al. J Am Chem Soc 76 1045 1954, NMR: Müller et al. J Am Chem Soc 78 3557 1956, Van Wazer et al. J Am Chem Soc 78 5715 1956, IR: Daasch & Smith Anal Chem 23 853 1951, Beilstein 16 IV 1074.]

Phenylphosphonic dichloride Preparation Products And Raw materials

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