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(-)-Sparteine sulfate pentahydrate

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(-)-Sparteine sulfate pentahydrate Basic information
(-)-Sparteine sulfate pentahydrate Chemical Properties
  • Melting point:133-140 °C(lit.)
  • alpha -28 º (589nm, c=2, H2O 25 ºC)
  • refractive index -22 ° (C=5, H2O)
  • storage temp. 2-8°C
  • solubility H2O: 0.1 g/mL, clear, colorless
  • Merck 8737
  • CAS DataBase Reference6160-12-9
Safety Information
  • Hazard Codes Xn
  • Risk Statements 22-20/21/22
  • Safety Statements 36-24/25
  • WGK Germany 3
  • RTECS WG6430000
  • HS Code 29399900
MSDS
(-)-Sparteine sulfate pentahydrate Usage And Synthesis
  • Chemical Propertieswhite fine crystalline powder
  • Usesoxytocic
  • Purification MethodsRecrystallise the sulfate from aqueous EtOH or H2O, although the solubility in the latter is high. The free (-)-base has b 173o/8mm and is steam volatile but resinifies in air. The dipicrate forms yellow needles from EtOH/Me2CO, m 205-206o [Clemo et al. J Chem Soc 429 1931; see also Bolnmann & Schuman The Alkaloids (Ed Manske) Vol 9 175 1967]. The free (±)-base has m 71-72.5o [van Tamelen & Foltz J Am Chem Soc 82 2400 1960]. [Beilstein 23 II 99, 23 III/IV 18.]
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