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MassMS-NW-4928 trichlorophenylsilane C6H5Cl3Si (Mass of molecular ion: 210)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
26.0 1.0 27.0 3.8 28.0 1.4 36.0 3.6 37.0 1.0 38.0 1.8 39.0 4.6 50.0 18.9 51.0 46.0 52.0 4.3 53.0 2.8 63.0 18.4 64.0 1.1 65.0 6.6 73.0 1.0 74.0 4.5 75.0 4.8 76.0 11.0 77.0 42.9 78.0 4.1 98.0 2.0 100.0 1.4 112.0 18.5 113.0 1.4 114.0 5.9 123.0 3.4 125.0 2.4 133.0 17.1 135.0 16.9 136.0 1.0 137.0 6.0 139.0 3.0 140.0 1.0 141.0 1.2 147.0 1.6 149.0 1.7 173.0 1.2 174.0 11.2 175.0 100.0 176.0 19.2 177.0 67.3 178.0 9.2 179.0 12.7 180.0 1.5 210.0 82.9 211.0 10.3 212.0 82.5 213.0 9.6 214.0 28.4 215.0 3.3 216.0 3.7
90 MHz in CDCl3
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1H NMR 89.56 MHz C6 H5 Cl3 Si 0.04 ml : 0.5 ml CDCl3 trichlorophenylsilane 
Assign. Shift(ppm)
A 7.78 B 7.65 to 7.34
Hz ppm Int.707.25 7.897 40 705.63 7.879 79 705.19 7.874 74 702.94 7.849 513 700.94 7.827 656 699.63 7.812 223 698.63 7.801 321 698.19 7.796 407 696.50 7.777 572 696.06 7.772 458 695.56 7.767 423 694.25 7.752 435 693.25 7.741 925 691.88 7.726 225 690.25 7.708 78 689.56 7.700 102 687.44 7.676 88 686.19 7.662 48 685.50 7.655 85 684.13 7.639 55 683.56 7.633 96 682.06 7.616 42 681.44 7.609 43 678.94 7.581 227 677.81 7.569 251 677.13 7.561 275 675.94 7.548 279 674.63 7.533 734 673.81 7.524 1000 673.44 7.520 912 672.63 7.511 879 672.25 7.507 991 671.44 7.498 625 670.94 7.492 496 669.63 7.477 433 668.25 7.462 490 667.56 7.454 491 666.63 7.444 536 666.25 7.440 517 663.69 7.411 146 662.88 7.402 135 661.56 7.387 210 659.44 7.364 88 658.19 7.350 71 657.38 7.341 88
in CDCl3
liquid film
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