-
MassMS-NW-4931 trichloro(3-chloropropyl)silane C3H6Cl4Si (Mass of molecular ion: 210)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
26.0 1.1 27.0 6.5 28.0 1.8 36.0 3.2 38.0 1.0 39.0 11.4 40.0 3.5 41.0 22.2 42.0 100.0 43.0 3.7 49.0 3.1 51.0 1.0 63.0 7.2 65.0 2.6 98.0 2.8 99.0 1.6 100.0 2.1 101.0 1.2 112.0 2.2 114.0 1.6 125.0 1.1 133.0 52.6 134.0 2.8 135.0 50.0 136.0 2.6 137.0 17.9 138.0 7.6 139.0 3.2 140.0 5.2 141.0 1.3 142.0 1.1 161.0 22.2 162.0 1.8 163.0 21.6 164.0 1.7 165.0 7.8 167.0 1.0 174.0 3.1 175.0 2.1 176.0 3.2 177.0 2.0 178.0 1.2
90 MHz in CDCl3
-
1H NMR 89.56 MHz C3 H6 Cl4 Si 0.04 ml : 0.5 ml CDCl3 trichloro(3-chloropropyl)silane 
Assign. Shift(ppm)
A 3.593 B 2.042 C 1.589
Hz ppm Int.328.44 3.668 471 326.75 3.649 129 324.19 3.620 133 322.38 3.600 1000 319.44 3.567 95 316.06 3.530 644 313.56 3.502 53 199.50 2.228 80 198.44 2.216 81 193.44 2.160 157 192.00 2.144 189 190.69 2.130 123 189.50 2.116 58 187.13 2.090 197 186.50 2.083 214 185.44 2.071 127 184.19 2.057 202 183.25 2.047 196 182.63 2.040 187 181.50 2.027 147 180.44 2.015 226 177.00 1.977 400 174.56 1.950 110 173.88 1.942 99 172.38 1.925 95 170.75 1.907 134 168.88 1.886 73 167.44 1.870 96 156.25 1.745 46 151.44 1.691 106 147.81 1.651 717 146.50 1.636 126 144.56 1.615 234 144.00 1.608 236 140.56 1.570 301 138.50 1.547 295 137.63 1.537 277 136.50 1.525 101 135.44 1.513 52 132.81 1.483 230 131.25 1.466 260 129.94 1.451 39
liquid film
更多供应商
