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MassMS-NW-3279 trichloro(propyl)silane C3H7Cl3Si (Mass of molecular ion: 176)
Source Temperature: 280 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 1.4 26.0 1.9 27.0 14.9 28.0 3.4 29.0 12.2 38.0 1.7 39.0 13.4 40.0 2.6 41.0 22.7 42.0 32.6 43.0 61.1 44.0 2.1 49.0 1.9 53.0 1.0 63.0 18.5 64.0 1.5 65.0 6.8 98.0 7.7 99.0 5.9 100.0 5.6 101.0 4.2 102.0 1.2 112.0 11.7 113.0 3.3 114.0 8.0 115.0 2.2 116.0 1.7 125.0 15.0 126.0 2.0 127.0 10.0 128.0 1.1 129.0 1.9 133.0 64.2 134.0 3.4 135.0 63.5 136.0 3.5 137.0 21.8 138.0 1.3 139.0 3.7 140.0 100.0 141.0 11.0 142.0 67.5 143.0 6.7 144.0 12.6 145.0 1.3 161.0 22.0 162.0 1.9 163.0 21.7 164.0 1.8 165.0 7.5 167.0 1.0 175.0 1.2 176.0 3.8 177.0 1.5 178.0 3.9 180.0 1.4
400 MHz in CDCl3
90 MHz in CDCl3
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1H NMR 399.65 MHz C3 H7 Cl3 Si 0.05 ml : 0.5 ml CDCl3 trichloro(propyl)silane 
Assign. Shift(ppm)
A 1.641 B 1.403 C 1.072
Hz ppm Int.676.15 1.692 33 675.17 1.690 34 670.78 1.679 30 668.58 1.673 113 667.97 1.672 104 665.16 1.665 44 663.57 1.661 65 660.89 1.654 183 657.71 1.646 80 656.25 1.643 89 654.66 1.639 93 653.44 1.636 157 652.22 1.632 179 650.39 1.628 78 648.93 1.624 66 647.46 1.621 43 645.02 1.614 142 643.19 1.610 39 638.06 1.597 45 637.21 1.595 44 571.78 1.431 30 567.63 1.421 370 563.35 1.410 117 561.89 1.406 206 559.45 1.400 264 558.84 1.399 264 557.62 1.396 164 556.15 1.392 127 551.64 1.381 230 551.03 1.379 237 435.06 1.089 614 427.86 1.071 1000 423.34 1.060 35 420.41 1.052 520
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1H NMR 89.56 MHz C3 H7 Cl3 Si 0.04 ml : 0.5 ml CDCl3 trichloro(propyl)silane Assign. Shift(ppm)
A 1.61 B 1.41 C 1.07
Hz ppm Int.162.38 1.814 32 161.69 1.806 41 158.63 1.772 62 156.19 1.744 38 155.25 1.734 67 154.69 1.728 79 153.25 1.712 63 152.75 1.706 51 151.50 1.692 139 149.38 1.668 123 147.81 1.651 76 146.19 1.633 126 145.75 1.628 104 145.00 1.620 151 144.06 1.609 196 142.00 1.586 126 140.56 1.570 86 140.00 1.564 112 138.94 1.552 186 137.25 1.533 200 135.44 1.513 75 133.81 1.495 137 132.88 1.484 237 131.88 1.473 312 131.25 1.466 275 130.50 1.458 272 129.44 1.446 149 128.25 1.433 122 127.38 1.423 189 125.88 1.406 74 125.06 1.397 173 123.31 1.377 123 122.81 1.372 132 122.44 1.368 140 121.50 1.357 108 119.75 1.338 47 117.75 1.315 148 115.44 1.289 88 115.06 1.285 86 103.19 1.153 172 102.44 1.144 330 101.75 1.137 403 100.88 1.127 175 100.25 1.120 124 95.75 1.070 1000 92.88 1.038 85 89.13 0.996 181 88.44 0.988 280 86.63 0.968 69
in CDCl3
liquid film
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