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网站主页CAS数据库列表 92-06-8更多图谱间三联苯(92-06-8)核磁图(13CNMR)

间三联苯

产品名称 间三联苯

CAS号92-06-8

分子式C18H14

分子量230.3

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  • Mass

    MS-NW-8176          
    m-terphenyl
    C18H14              (Mass of molecular ion:    230)
    

       Source Temperature: 160 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          51.0       1.4
          63.0       1.1
          75.0       1.0
          76.0       1.5
          77.0       1.1
          88.0       1.7
          89.0       1.2
          94.5       1.0
         100.0       1.2
         101.0       4.5
         102.0       1.2
         107.5       1.3
         113.0       3.3
         113.5       1.1
         114.0       2.6
         115.0       9.1
         115.5       1.5
         128.0       1.6
         151.0       2.0
         152.0       3.8
         153.0       1.7
         189.0       1.2
         202.0       4.2
         203.0       1.6
         215.0       3.5
         226.0       5.2
         227.0       4.7
         228.0      11.8
         229.0      10.4
         230.0     100.0
         231.0      19.6
         232.0       1.7
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C18 H14 16.4 mg : 0.5 ml CDCl3
    m-terphenyl
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.808 B 7.647 C 7.572 D 7.512 E 7.458 F 7.370 J(A,C)=2.1HZ. J(A,D)=0.7HZ.

         Hz     ppm     Int.
    

       3122.68   7.814    180
       3122.19   7.813    185
       3120.85   7.809    358
       3120.36   7.808    329
       3119.02   7.805    223
       3118.53   7.804    184
       3068.97   7.680     30
       3068.12   7.678     34
       3066.04   7.672     41
       3065.43   7.671     44
       3061.52   7.661    655
       3060.18   7.658    862
       3058.11   7.652    331
       3053.96   7.642    441
       3053.10   7.640    930
       3052.37   7.638    716
       3051.88   7.637    779
       3050.90   7.634    240
       3049.80   7.632    226
       3033.08   7.590    203
       3031.37   7.586    351
       3029.54   7.581    227
       3028.08   7.577     42
       3027.71   7.576     42
       3025.02   7.570    441
       3024.41   7.568    449
       3023.19   7.565    456
       3022.58   7.564    419
       3008.18   7.528    297
       3007.69   7.526    261
       3001.71   7.511    194
       3001.22   7.510    177
       2999.51   7.506    145
       2998.90   7.504    126
       2993.04   7.490    124
       2992.55   7.488    113
       2990.36   7.483    152
       2989.38   7.480    354
       2988.53   7.478    491
       2986.82   7.474    209
       2981.32   7.460   1000
       2980.10   7.457    523
       2975.10   7.445    305
       2973.51   7.441    567
       2971.56   7.436    130
       2952.51   7.388    223
       2951.17   7.385    404
       2949.95   7.382    227
       2945.80   7.371    178
       2943.85   7.367    433
       2941.77   7.361    152
       2937.74   7.351    126
       2936.52   7.348    192
       2935.18   7.345    103
       2934.20   7.342     34
    


  • 1H NMR 89.56 MHz
    C18 H14 0.016 g : 0.5 ml CDCl3
    m-terphenyl
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.80 B 7.64 C 7.58 to 7.23

         Hz     ppm     Int.
    

        700.88   7.826    115
        699.63   7.812    206
        698.94   7.805    184
        698.38   7.798    269
        697.38   7.787    187
        696.63   7.779    173
        690.06   7.706    278
        687.88   7.681    306
        686.50   7.666    736
        685.56   7.655    222
        684.56   7.644    238
        684.00   7.638    282
        682.69   7.623    258
        681.94   7.615    755
        680.06   7.594    899
        678.06   7.572    264
        676.81   7.558    690
        676.44   7.553    670
        675.13   7.539   1000
        674.25   7.529    508
        673.56   7.521    306
        672.94   7.514    389
        671.88   7.503    248
        671.31   7.496    322
        668.63   7.466    615
        667.75   7.456    669
        665.94   7.436    322
        664.50   7.420    393
        662.00   7.392    866
        660.56   7.376    799
        657.13   7.338    199
        655.63   7.321    146
    

in CDCl3



CCl4 solution



KBr disc



nujol mull





ANION RADICAL, REDUCTION WITH LI OR NA METAL