二苯基氯化膦

Mass

MS-NW-3723          
chlorodiphenylphosphine
C12H10ClP           (Mass of molecular ion:    220)

   Source Temperature: 270 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      27.0       2.2
      39.0       5.0
      50.0       5.5
      51.0      18.6
      52.0       1.5
      56.0       2.4
      57.0       4.5
      63.0       3.1
      65.0       1.6
      68.0       1.1
      69.0       1.3
      74.0       1.9
      75.0       1.7
      76.0       1.9
      77.0      10.9
      78.0       1.7
      80.0       2.8
      81.0       5.2
      82.0       1.7
      83.0       1.3
      91.0       2.0
      91.5       1.8
      92.0       5.0
     102.0       1.0
     107.0      29.3
     108.0      12.8
     109.0       1.4
     115.0       3.1
     128.0       1.4
     133.0       2.4
     139.0       1.6
     141.0       1.3
     143.0      29.4
     144.0       2.3
     145.0       9.7
     151.0       1.2
     152.0       8.4
     153.0       6.3
     154.0     100.0
     155.0      13.3
     157.0       3.4
     170.0       2.1
     181.0       1.4
     183.0      51.9
     184.0      20.5
     185.0      18.9
     186.0       3.5
     219.0      11.3
     220.0      90.2
     221.0      15.4
     222.0      30.1
     223.0       4.0
     235.0       1.3
     264.0       1.7
     266.0       1.9

Assign. Shift(ppm) A 7.57 B 7.47 to 7.25

     Hz     ppm     Int.

    687.69   7.679    148
    685.94   7.660    127
    685.44   7.654    140
    684.56   7.644    188
    683.75   7.635    153
    683.25   7.629    142
    682.19   7.618    201
    680.81   7.602    311
    679.44   7.587    233
    678.00   7.571    485
    677.00   7.560    298
    676.13   7.550    261
    674.13   7.528    355
    673.19   7.517    312
    671.50   7.498    277
    670.31   7.485    416
    668.69   7.467    236
    666.44   7.442    208
    664.44   7.419    349
    662.88   7.402    757
    661.50   7.387   1000
    659.88   7.369    727
    658.63   7.355    812
    656.44   7.330    608
    654.81   7.312    414
    652.69   7.288    113