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网站主页CAS数据库列表 1079-66-9更多图谱二苯基氯化膦(1079-66-9)核磁图(13CNMR)

二苯基氯化膦

产品名称 二苯基氯化膦

CAS号1079-66-9

分子式C12H10ClP

分子量220.63

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  • Mass

    MS-NW-3723          
    chlorodiphenylphosphine
    C12H10ClP           (Mass of molecular ion:    220)
    

       Source Temperature: 270 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          27.0       2.2
          39.0       5.0
          50.0       5.5
          51.0      18.6
          52.0       1.5
          56.0       2.4
          57.0       4.5
          63.0       3.1
          65.0       1.6
          68.0       1.1
          69.0       1.3
          74.0       1.9
          75.0       1.7
          76.0       1.9
          77.0      10.9
          78.0       1.7
          80.0       2.8
          81.0       5.2
          82.0       1.7
          83.0       1.3
          91.0       2.0
          91.5       1.8
          92.0       5.0
         102.0       1.0
         107.0      29.3
         108.0      12.8
         109.0       1.4
         115.0       3.1
         128.0       1.4
         133.0       2.4
         139.0       1.6
         141.0       1.3
         143.0      29.4
         144.0       2.3
         145.0       9.7
         151.0       1.2
         152.0       8.4
         153.0       6.3
         154.0     100.0
         155.0      13.3
         157.0       3.4
         170.0       2.1
         181.0       1.4
         183.0      51.9
         184.0      20.5
         185.0      18.9
         186.0       3.5
         219.0      11.3
         220.0      90.2
         221.0      15.4
         222.0      30.1
         223.0       4.0
         235.0       1.3
         264.0       1.7
         266.0       1.9
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C12 H10 Cl P 0.04 ml : 0.5 ml CDCl3
    chlorodiphenylphosphine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.57 B 7.47 to 7.25

         Hz     ppm     Int.
    

        687.69   7.679    148
        685.94   7.660    127
        685.44   7.654    140
        684.56   7.644    188
        683.75   7.635    153
        683.25   7.629    142
        682.19   7.618    201
        680.81   7.602    311
        679.44   7.587    233
        678.00   7.571    485
        677.00   7.560    298
        676.13   7.550    261
        674.13   7.528    355
        673.19   7.517    312
        671.50   7.498    277
        670.31   7.485    416
        668.69   7.467    236
        666.44   7.442    208
        664.44   7.419    349
        662.88   7.402    757
        661.50   7.387   1000
        659.88   7.369    727
        658.63   7.355    812
        656.44   7.330    608
        654.81   7.312    414
        652.69   7.288    113
    

in CDCl3



liquid film