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MassMS-NW-5281 dichlorodiphenylsilane C12H10Cl2Si (Mass of molecular ion: 252)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
27.0 1.2 39.0 1.6 50.0 5.1 51.0 15.4 52.0 1.4 53.0 1.7 63.0 15.9 65.0 5.7 74.0 1.8 75.0 1.8 76.0 4.6 77.0 28.0 78.0 3.0 108.0 6.6 108.5 1.5 109.0 2.5 123.0 1.7 125.0 1.1 139.0 3.0 140.0 1.0 141.0 1.4 151.0 1.6 152.0 5.6 153.0 5.4 154.0 100.0 155.0 13.3 174.0 1.6 175.0 35.2 176.0 5.3 177.0 23.5 178.0 3.0 179.0 4.6 180.0 1.0 181.0 2.3 215.0 9.8 216.0 7.6 217.0 10.2 218.0 3.7 219.0 2.7 251.0 2.6 252.0 34.4 253.0 7.9 254.0 23.4 255.0 4.7 256.0 4.7
90 MHz in CDCl3
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1H NMR 89.56 MHz C12 H10 Cl2 Si 0.04 ml : 0.5 ml CDCl3 dichlorodiphenylsilane 
Assign. Shift(ppm)
A 7.74 B 7.51 C 7.47
Hz ppm Int.701.31 7.831 52 700.19 7.819 44 698.63 7.801 452 696.44 7.777 597 695.19 7.763 154 693.75 7.747 410 692.31 7.731 508 691.88 7.726 373 691.31 7.719 314 690.00 7.705 415 688.94 7.693 772 687.31 7.675 147 685.69 7.657 91 683.56 7.633 75 681.63 7.611 76 680.38 7.597 43 679.56 7.588 69 675.19 7.539 180 674.06 7.527 192 673.13 7.516 262 671.06 7.493 885 670.50 7.487 1000 668.75 7.468 989 668.19 7.461 750 665.88 7.436 366 665.25 7.428 442 664.56 7.421 432 663.50 7.409 516 662.38 7.396 143 660.00 7.370 96 658.75 7.356 168 657.50 7.342 76 656.25 7.328 65 655.13 7.315 48 654.19 7.305 60
in CDCl3
liquid film
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