图谱信息 供应商 相关产品
网站主页CAS数据库列表 102-08-9更多图谱N,N'-二苯基硫脲(102-08-9)红外图谱(IR2)

N,N'-二苯基硫脲

产品名称 N,N'-二苯基硫脲

CAS号102-08-9

分子式C13H12N2S

分子量228.31

展开


  • Mass

    MS-NW-8144          
    1,3-diphenylthiourea
    C13H12N2S           (Mass of molecular ion:    228)
    

       Source Temperature: 170 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          18.0       4.3
          27.0       1.7
          28.0       3.3
          32.0       1.3
          34.0       2.4
          37.0       1.2
          38.0       2.6
          39.0       8.3
          40.0       2.1
          41.0       1.9
          46.5       1.8
          50.0       6.3
          51.0      22.5
          52.0       3.3
          54.0       1.6
          62.0       1.2
          63.0       3.9
          64.0       4.3
          65.0      13.0
          66.0      18.5
          67.0       2.0
          67.5       2.3
          74.0       1.8
          75.0       1.8
          76.0       3.3
          77.0      51.4
          78.0       4.9
          90.0       1.1
          91.0       7.6
          92.0       9.8
          93.0     100.0
          94.0       7.0
          97.0       1.0
         103.0       1.7
         104.0       1.5
         108.0       1.7
         109.0       5.5
         110.0       4.1
         114.0       1.7
         118.0       2.6
         119.0       5.1
         124.0       1.0
         135.0      36.9
         136.0       9.4
         137.0       2.3
         193.0       1.2
         194.0      19.1
         195.0       5.8
         227.0       4.1
         228.0      21.6
         229.0       3.5
         230.0       1.2
    

400 MHz in DMSO-d6

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C13 H12 N2 S 0.036 g : 0.5 ml DMSO-d6
    1,3-diphenylthiourea
    ChemicalStructure
        Assign.     Shift(ppm)
    A 9.75 B 7.496 C 7.326 D 7.122

         Hz     ppm     Int.
    

       3895.77   9.748    586
       3001.18   7.510    655
       2999.90   7.507    840
       2992.57   7.488    974
       2991.66   7.486    940
       2937.81   7.351    155
       2935.98   7.347    704
       2933.96   7.342    293
       2928.47   7.328   1000
       2921.87   7.312    309
       2920.04   7.307    704
       2918.03   7.302    167
       2854.47   7.143    210
       2853.37   7.140    376
       2852.27   7.137    252
       2846.04   7.122    606
       2839.81   7.106    179
       2838.71   7.103    275
       2837.43   7.100    175
    


  • 1H NMR 89.56 MHz
    C13 H12 N2 S 0.039 g : 0.5 ml CDCl3
    1,3-diphenylthiourea
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.2 B 7.43 to 7.22

         Hz     ppm     Int.
    

        733.00   8.185     53
        665.88   7.436     28
        663.00   7.403    176
        660.88   7.380    144
        659.13   7.360   1000
        656.56   7.331    123
        655.38   7.318    133
        653.00   7.292     86
        651.56   7.276     51
        650.19   7.260     41
        649.38   7.251     63
        648.38   7.240     23
        646.94   7.224     39
    

in DMSO-d6

in CDCl3





KBr disc



nujol mull