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网站主页CAS数据库列表 137-97-3更多图谱N,N'-二邻甲苯基硫脲(137-97-3)红外图谱(IR2)

N,N'-二邻甲苯基硫脲

产品名称 N,N'-二邻甲苯基硫脲

CAS号137-97-3

分子式C15H16N2S

分子量256.37

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  • Mass

    MS-NW-0475          
    1,3-di(o-tolyl)-2-thiourea
    C15H16N2S           (Mass of molecular ion:    256)
    

       Source Temperature: 210 °C
       Sample Temperature: 140 °C
       Direct, 75 eV
    

          27.0       3.2
          28.0       3.0
          30.0       1.8
          32.0       1.3
          33.0       1.0
          34.0       2.7
          38.0       1.9
          39.0      13.0
          40.0       1.3
          41.0       3.5
          45.0       4.1
          50.0       3.6
          51.0       8.5
          52.0       4.5
          53.0       2.6
          54.0       1.1
          62.0       1.9
          63.0       7.4
          64.0       3.1
          65.0      21.2
          66.0       1.9
          75.0       1.2
          76.0       1.5
          77.0      13.7
          78.0       7.8
          79.0       8.0
          80.0       2.7
          89.0       9.5
          90.0       7.4
          91.0      30.6
          92.0       3.3
          93.0       1.6
         103.0       1.1
         104.0       7.8
         105.0       2.5
         106.0      53.9
         107.0     100.0
         108.0       8.2
         116.0       6.7
         117.0      18.1
         118.0       3.5
         121.0       4.8
         122.0       1.6
         123.0       3.2
         124.0       7.0
         127.0       1.1
         128.0       1.1
         130.0       6.5
         131.0       4.2
         132.0       3.3
         133.0       6.0
         148.0       8.4
         149.0      27.9
         150.0      11.3
         151.0       2.4
         165.0       1.0
         204.0       1.9
         205.0       1.7
         206.0       2.7
         207.0       3.9
         208.0       1.0
         221.0      10.5
         222.0      25.9
         223.0      14.4
         224.0       2.4
         241.0      19.4
         242.0       3.6
         243.0       1.3
         255.0       5.5
         256.0      42.1
         257.0       7.9
         258.0       2.5
    

90 MHz in CDCl3

400 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C15 H16 N2 S 0.039 g : 0.5 ml CDCl3
    1,3-di(o-tolyl)-2-thiourea
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.7 B 7.36 C 7.27 to 7.200 D 2.294 400MHZ : HSP-44-178

         Hz     ppm     Int.
    

        692.69   7.735     54
        667.06   7.449     28
        664.81   7.424     37
        662.75   7.401     57
        661.81   7.390     55
        659.56   7.365     93
        656.75   7.334    108
        654.63   7.310     81
        651.50   7.275    165
        649.06   7.248    625
        647.13   7.226    214
        645.75   7.211    264
        641.94   7.168     44
        639.94   7.146     52
        205.50   2.295   1000
        200.13   2.235     30
    


  • 1H NMR 399.65 MHz
    C15 H16 N2 S 0.033 g : 0.5 ml CDCl3
    1,3-di(o-tolyl)-2-thiourea
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.8 B 7.379 C 7.27 to 7.22 D 2.299 90MHZ : HSP-04-941

         Hz     ppm     Int.
    

       2957.40   7.400     34
       2953.37   7.390    172
       2950.20   7.382    192
       2948.49   7.378    120
       2944.58   7.368    203
       2941.53   7.361     31
       2941.16   7.360     31
       2907.10   7.275     88
       2899.05   7.254    540
       2895.26   7.245    433
       2893.68   7.241    418
       2890.14   7.232    468
       2887.33   7.225    161
       2885.50   7.221    196
       2880.13   7.207     34
        934.45   2.339     32
        931.52   2.331     39
        918.95   2.300   1000
    

in CDCl3



KBr disc



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