二苯氨基脲

Mass

MS-NW-0393          
1,5-diphenylcarbonohydrazide
C13H14N4O           (Mass of molecular ion:    242)

   Source Temperature: 200 °C
   Sample Temperature: 140 °C
   Direct, 75 eV

      18.0       1.5
      27.0       1.6
      28.0       1.9
      29.0       3.2
      37.0       1.2
      38.0       2.8
      39.0       9.6
      40.0       1.4
      41.0       1.4
      43.0       2.2
      44.0       9.2
      46.5       1.0
      50.0       4.8
      51.0      15.7
      52.0       4.6
      53.0       2.0
      54.0       1.0
      62.0       1.1
      63.0       3.9
      64.0       4.6
      65.0      21.8
      66.0       8.6
      67.0       1.1
      74.0       1.3
      76.0       1.6
      77.0      47.8
      78.0      14.5
      79.0       5.8
      80.0       4.1
      91.0      11.7
      92.0      31.4
      93.0     100.0
      94.0      10.7
     105.0       6.8
     106.0       9.4
     107.0      34.5
     108.0      77.8
     109.0       5.9
     134.0       3.2
     150.0       2.9
     151.0      36.9
     152.0       3.2
     242.0      11.2
     243.0       1.7

Assign. Shift(ppm) A *1 8.28 B *1 7.53 C 7.141 D 6.73 E 6.70

     Hz     ppm     Int.

   3325.81   8.322     22
   3323.36   8.316     27
   3322.63   8.314     30
   3307.86   8.277    254
   3292.97   8.240     27
   3291.50   8.236     22
   3024.90   7.569     23
   3023.93   7.567     25
   3009.77   7.532    370
   2861.57   7.161    484
   2853.64   7.141    832
   2845.95   7.122    554
   2839.11   7.104     23
   2703.61   6.765     23
   2702.88   6.764     26
   2692.75   6.738    885
   2684.94   6.719   1000
   2676.88   6.699    497
   2669.68   6.681    238