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网站主页CAS数据库列表 100-63-0更多图谱苯肼(100-63-0)红外图谱(IR2)

苯肼

产品名称 苯肼

CAS号100-63-0

分子式C6H8N2

分子量108.14

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  • Mass

    MS-NW-1086          
    phenylhydrazine
    C6H8N2              (Mass of molecular ion:    108)
    

       Source Temperature: 240 °C
       Sample Temperature: 170 °C
       Reservoir, 75 eV
    

          16.0       2.2
          17.0       3.0
          18.0       6.2
          26.0       2.0
          27.0       5.5
          28.0      18.1
          29.0       4.7
          30.0       1.3
          31.0       2.6
          37.0       5.0
          38.0       8.5
          39.0      22.7
          40.0       3.3
          41.0       5.2
          46.5       1.0
          49.0       2.2
          50.0      17.5
          51.0      40.6
          52.0      14.3
          53.0       3.7
          54.0       4.0
          61.0       2.0
          62.0       2.9
          63.0       8.8
          64.0       9.7
          65.0      46.4
          66.0      12.7
          67.0       1.7
          69.0       2.8
          73.0       1.6
          74.0       5.2
          75.0       2.9
          76.0       3.7
          77.0      84.3
          78.0      47.1
          79.0      12.2
          80.0       4.5
          81.0       1.6
          87.0       1.2
          90.0       1.0
          91.0      16.8
          92.0      44.0
          93.0      35.0
          94.0       2.5
         105.0      10.6
         106.0      29.5
         107.0       6.9
         108.0     100.0
         109.0       7.2
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C6 H8 N2 0.04 ml : 0.5 ml CDCl3
    phenylhydrazine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.21 B 6.80 C 6.76 D 4.0

         Hz     ppm     Int.
    

        655.13   7.315    259
        654.31   7.306    322
        652.44   7.285    198
        649.50   7.253     93
        648.69   7.244    212
        647.94   7.235    411
        647.44   7.230    276
        646.88   7.223    452
        646.06   7.214    514
        645.13   7.204    383
        644.06   7.192    111
        641.81   7.167    208
        639.75   7.144    361
        639.25   7.138    546
        638.56   7.130    603
        636.69   7.110    140
        617.00   6.890    133
        616.00   6.879    214
        615.50   6.873    284
        614.50   6.862    429
        611.75   6.831    230
        610.13   6.813    744
        609.50   6.806   1000
        609.13   6.802    978
        607.44   6.783    837
        603.63   6.740    250
        603.13   6.735    238
        602.38   6.726    223
        601.81   6.720    605
        601.06   6.712    799
        600.56   6.706    596
        599.81   6.698    136
        598.06   6.678     76
        358.00   3.998    175
    

in CDCl3



CCl4 solution



liquid film