苯肼

Mass

MS-NW-1086          
phenylhydrazine
C6H8N2              (Mass of molecular ion:    108)

   Source Temperature: 240 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      16.0       2.2
      17.0       3.0
      18.0       6.2
      26.0       2.0
      27.0       5.5
      28.0      18.1
      29.0       4.7
      30.0       1.3
      31.0       2.6
      37.0       5.0
      38.0       8.5
      39.0      22.7
      40.0       3.3
      41.0       5.2
      46.5       1.0
      49.0       2.2
      50.0      17.5
      51.0      40.6
      52.0      14.3
      53.0       3.7
      54.0       4.0
      61.0       2.0
      62.0       2.9
      63.0       8.8
      64.0       9.7
      65.0      46.4
      66.0      12.7
      67.0       1.7
      69.0       2.8
      73.0       1.6
      74.0       5.2
      75.0       2.9
      76.0       3.7
      77.0      84.3
      78.0      47.1
      79.0      12.2
      80.0       4.5
      81.0       1.6
      87.0       1.2
      90.0       1.0
      91.0      16.8
      92.0      44.0
      93.0      35.0
      94.0       2.5
     105.0      10.6
     106.0      29.5
     107.0       6.9
     108.0     100.0
     109.0       7.2

Assign. Shift(ppm) A 7.21 B 6.80 C 6.76 D 4.0

     Hz     ppm     Int.

    655.13   7.315    259
    654.31   7.306    322
    652.44   7.285    198
    649.50   7.253     93
    648.69   7.244    212
    647.94   7.235    411
    647.44   7.230    276
    646.88   7.223    452
    646.06   7.214    514
    645.13   7.204    383
    644.06   7.192    111
    641.81   7.167    208
    639.75   7.144    361
    639.25   7.138    546
    638.56   7.130    603
    636.69   7.110    140
    617.00   6.890    133
    616.00   6.879    214
    615.50   6.873    284
    614.50   6.862    429
    611.75   6.831    230
    610.13   6.813    744
    609.50   6.806   1000
    609.13   6.802    978
    607.44   6.783    837
    603.63   6.740    250
    603.13   6.735    238
    602.38   6.726    223
    601.81   6.720    605
    601.06   6.712    799
    600.56   6.706    596
    599.81   6.698    136
    598.06   6.678     76
    358.00   3.998    175