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MS-IW-7588 dichloromethyloctylsilane C9H20Cl2Si (Mass of molecular ion: 226)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 5.0 28.0 1.1 29.0 8.7 36.0 1.1 39.0 4.0 41.0 16.3 42.0 6.0 43.0 44.6 44.0 1.5 53.0 1.1 54.0 1.5 55.0 9.4 56.0 13.2 57.0 26.4 58.0 1.1 63.0 4.7 65.0 1.9 67.0 1.0 68.0 1.2 69.0 8.4 70.0 11.3 71.0 11.9 78.0 1.6 79.0 4.3 81.0 1.6 82.0 2.8 83.0 9.1 84.0 11.4 85.0 14.7 86.0 1.0 92.0 1.0 93.0 1.6 97.0 2.1 99.0 1.8 101.0 1.1 105.0 1.6 107.0 1.2 111.0 1.0 112.0 17.5 113.0 100.0 114.0 7.4 115.0 69.0 116.0 4.4 117.0 13.1 119.0 2.8 121.0 1.1 125.0 1.1 127.0 1.4 133.0 1.7 134.0 1.2 141.0 62.1 142.0 5.5 143.0 42.1 144.0 3.5 145.0 7.8 147.0 8.2 148.0 1.2 149.0 3.0 155.0 8.4 156.0 1.2 157.0 5.7 159.0 1.1 161.0 3.1 162.0 1.2 163.0 1.2 167.0 1.4 169.0 4.6 171.0 2.7 183.0 2.0 185.0 1.3 190.0 3.0 191.0 1.5 192.0 1.2 197.0 1.1 211.0 10.5 212.0 1.5 213.0 7.1 214.0 1.0 215.0 1.3 226.0 6.3 228.0 4.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C9 H20 Cl2 Si 0.05 ml : 0.5 ml CDCl3 dichloromethyloctylsilane Assign. Shift(ppm)
A 1.504 B 1.37 C 1.28 D 1.110 E 0.885 F 0.759
Hz ppm Int.
609.13 1.525 39 608.64 1.523 39 606.45 1.518 30 601.07 1.504 65 599.85 1.501 58 598.51 1.498 39 597.05 1.494 32 595.34 1.490 44 593.02 1.484 75 590.09 1.477 40 585.33 1.465 34 584.23 1.462 31 556.03 1.392 43 554.08 1.387 38 553.34 1.385 38 548.83 1.374 56 545.17 1.365 42 541.99 1.357 47 537.23 1.345 34 534.91 1.339 37 529.91 1.326 49 523.44 1.310 101 514.89 1.289 197 510.74 1.278 300 451.42 1.130 156 446.04 1.117 59 442.87 1.109 87 441.65 1.106 67 435.06 1.089 129 360.72 0.903 109 354.00 0.886 363 346.92 0.869 148 307.25 0.769 44 303.47 0.760 1000 299.80 0.751 51
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