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网站主页CAS数据库列表 18407-07-3更多图谱甲基十二烷基二氯硅烷(18407-07-3)核磁图(13CNMR)

甲基十二烷基二氯硅烷

产品名称 甲基十二烷基二氯硅烷

CAS号18407-07-3

分子式C13H28Cl2Si

分子量283.35

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  • Mass

    MS-IW-7607          
    dichlorododecylmethylsilane
    C13H28Cl2Si         (Mass of molecular ion:    282)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          27.0       5.6
          28.0       1.2
          29.0      15.2
          36.0       2.0
          39.0       4.4
          41.0      31.2
          42.0       9.5
          43.0      74.0
          44.0       2.7
          53.0       1.8
          54.0       3.5
          55.0      22.7
          56.0      19.0
          57.0      91.1
          58.0       5.0
          63.0       3.3
          65.0       1.3
          67.0       2.7
          68.0       2.8
          69.0      19.2
          70.0      18.7
          71.0      64.4
          72.0       3.6
          78.0       1.7
          79.0       4.9
          81.0       1.9
          82.0       4.1
          83.0      12.8
          84.0      14.5
          85.0      44.9
          86.0       2.8
          93.0       1.7
          96.0       2.5
          97.0      11.1
          98.0      11.3
          99.0      12.8
         101.0       1.0
         105.0       1.8
         107.0       1.1
         110.0       1.3
         111.0       7.3
         112.0       6.8
         113.0     100.0
         114.0       7.3
         115.0      69.6
         116.0       4.5
         117.0      13.2
         119.0       3.4
         121.0       1.3
         125.0       3.6
         126.0       3.3
         127.0       2.6
         133.0       2.5
         135.0       1.0
         139.0       1.6
         140.0       4.7
         141.0      63.8
         142.0       5.6
         143.0      43.2
         144.0       3.6
         145.0       7.8
         147.0       9.5
         148.0       1.4
         149.0       3.4
         154.0       6.1
         155.0      31.0
         156.0       7.1
         157.0      20.9
         158.0       2.7
         159.0       4.0
         161.0       5.2
         163.0       1.9
         167.0       1.7
         168.0      12.0
         169.0      18.4
         170.0       2.7
         171.0      12.0
         172.0       1.3
         173.0       2.2
         182.0       1.1
         183.0       9.0
         184.0       1.7
         185.0       5.9
         187.0       1.1
         197.0       5.5
         198.0       1.0
         199.0       3.7
         211.0       3.1
         213.0       2.2
         225.0       3.0
         227.0       2.0
         239.0       2.6
         241.0       1.8
         246.0       2.6
         247.0       1.4
         248.0       1.1
         253.0       2.2
         255.0       1.6
         267.0       8.1
         268.0       1.6
         269.0       5.7
         270.0       1.0
         271.0       1.1
         282.0      10.5
         283.0       2.1
         284.0       7.3
         285.0       1.4
         286.0       1.4
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C13 H28 Cl2 Si 0.05 ml : 0.5 ml CDCl3
    dichlorododecylmethylsilane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 1.492 B 1.37 C 1.27 D 1.108 E 0.880 F 0.757

         Hz     ppm     Int.
    

        607.79   1.521     36
        600.10   1.502     60
        599.00   1.499     53
        596.19   1.492     32
        594.48   1.488     41
        592.16   1.482     66
        589.23   1.475     36
        584.47   1.463     30
        554.69   1.388     41
        547.61   1.371     55
        540.77   1.354     47
        540.41   1.353     47
        533.45   1.335     42
        520.75   1.304    104
        505.49   1.265   1000
        450.44   1.128    142
        445.07   1.114     56
        441.89   1.106     81
        434.08   1.087    115
        359.01   0.899    116
        352.29   0.882    360
        345.34   0.865    147
        302.61   0.758    966
    

in CDCl3



liquid film