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MS-IW-7607 dichlorododecylmethylsilane C13H28Cl2Si (Mass of molecular ion: 282)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 5.6 28.0 1.2 29.0 15.2 36.0 2.0 39.0 4.4 41.0 31.2 42.0 9.5 43.0 74.0 44.0 2.7 53.0 1.8 54.0 3.5 55.0 22.7 56.0 19.0 57.0 91.1 58.0 5.0 63.0 3.3 65.0 1.3 67.0 2.7 68.0 2.8 69.0 19.2 70.0 18.7 71.0 64.4 72.0 3.6 78.0 1.7 79.0 4.9 81.0 1.9 82.0 4.1 83.0 12.8 84.0 14.5 85.0 44.9 86.0 2.8 93.0 1.7 96.0 2.5 97.0 11.1 98.0 11.3 99.0 12.8 101.0 1.0 105.0 1.8 107.0 1.1 110.0 1.3 111.0 7.3 112.0 6.8 113.0 100.0 114.0 7.3 115.0 69.6 116.0 4.5 117.0 13.2 119.0 3.4 121.0 1.3 125.0 3.6 126.0 3.3 127.0 2.6 133.0 2.5 135.0 1.0 139.0 1.6 140.0 4.7 141.0 63.8 142.0 5.6 143.0 43.2 144.0 3.6 145.0 7.8 147.0 9.5 148.0 1.4 149.0 3.4 154.0 6.1 155.0 31.0 156.0 7.1 157.0 20.9 158.0 2.7 159.0 4.0 161.0 5.2 163.0 1.9 167.0 1.7 168.0 12.0 169.0 18.4 170.0 2.7 171.0 12.0 172.0 1.3 173.0 2.2 182.0 1.1 183.0 9.0 184.0 1.7 185.0 5.9 187.0 1.1 197.0 5.5 198.0 1.0 199.0 3.7 211.0 3.1 213.0 2.2 225.0 3.0 227.0 2.0 239.0 2.6 241.0 1.8 246.0 2.6 247.0 1.4 248.0 1.1 253.0 2.2 255.0 1.6 267.0 8.1 268.0 1.6 269.0 5.7 270.0 1.0 271.0 1.1 282.0 10.5 283.0 2.1 284.0 7.3 285.0 1.4 286.0 1.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C13 H28 Cl2 Si 0.05 ml : 0.5 ml CDCl3 dichlorododecylmethylsilane Assign. Shift(ppm)
A 1.492 B 1.37 C 1.27 D 1.108 E 0.880 F 0.757
Hz ppm Int.
607.79 1.521 36 600.10 1.502 60 599.00 1.499 53 596.19 1.492 32 594.48 1.488 41 592.16 1.482 66 589.23 1.475 36 584.47 1.463 30 554.69 1.388 41 547.61 1.371 55 540.77 1.354 47 540.41 1.353 47 533.45 1.335 42 520.75 1.304 104 505.49 1.265 1000 450.44 1.128 142 445.07 1.114 56 441.89 1.106 81 434.08 1.087 115 359.01 0.899 116 352.29 0.882 360 345.34 0.865 147 302.61 0.758 966
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