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甲基十八烷基二氯化硅烷

产品名称 甲基十八烷基二氯化硅烷

CAS号5157-75-5

分子式C19H40Cl2Si

分子量367.51

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  • Mass

    MS-IW-7610          
    dichloromethyloctadecylsilane
    C19H40Cl2Si         (Mass of molecular ion:    366)
    

       Source Temperature: 150 °C
       Sample Temperature: 130 °C
       Direct, 75 eV
    

          27.0       2.9
          28.0       1.1
          29.0      11.8
          36.0       2.9
          38.0       1.0
          39.0       2.4
          41.0      29.1
          42.0       8.3
          43.0      73.0
          44.0       2.6
          53.0       1.4
          54.0       3.9
          55.0      31.2
          56.0      19.5
          57.0     100.0
          58.0       5.8
          63.0       1.4
          67.0       3.9
          68.0       4.0
          69.0      23.8
          70.0      19.6
          71.0      91.7
          72.0       5.3
          78.0       1.0
          79.0       3.3
          81.0       2.2
          82.0       5.4
          83.0      19.1
          84.0      17.2
          85.0      69.9
          86.0       4.6
          93.0       1.5
          95.0       1.3
          96.0       3.4
          97.0      16.7
          98.0      16.6
          99.0      26.2
         100.0       1.9
         105.0       1.2
         110.0       1.9
         111.0      10.2
         112.0      15.1
         113.0      56.1
         114.0       4.0
         115.0      37.8
         116.0       2.3
         117.0       7.3
         119.0       2.2
         121.0       1.0
         124.0       1.2
         125.0       6.0
         126.0      12.8
         127.0      14.7
         128.0       1.4
         133.0       1.7
         139.0       3.1
         140.0      10.1
         141.0      26.8
         142.0       2.4
         143.0      18.1
         144.0       1.4
         145.0       3.3
         147.0       4.5
         149.0       1.8
         153.0       1.8
         154.0       9.8
         155.0      37.4
         156.0      10.0
         157.0      25.2
         158.0       3.5
         159.0       4.8
         161.0       2.7
         167.0       1.6
         168.0       5.2
         169.0      26.2
         170.0       4.2
         171.0      17.4
         172.0       1.9
         173.0       3.3
         182.0       3.8
         183.0      16.4
         184.0       3.0
         185.0      10.5
         186.0       1.4
         187.0       2.0
         196.0       2.2
         197.0      13.3
         198.0       2.3
         199.0       8.9
         200.0       1.2
         201.0       1.7
         209.0       1.1
         210.0       1.1
         211.0       9.2
         212.0       1.9
         213.0       6.0
         215.0       1.1
         224.0       2.0
         225.0       9.1
         226.0       2.3
         227.0       5.8
         228.0       1.0
         229.0       1.1
         238.0       1.8
         239.0       7.0
         240.0       2.3
         241.0       4.9
         252.0       6.8
         253.0       8.2
         254.0       2.9
         255.0       5.3
         256.0       1.1
         257.0       1.0
         266.0       2.3
         267.0       6.4
         268.0       2.7
         269.0       4.4
         270.0       1.0
         280.0       2.6
         281.0       7.7
         282.0       3.1
         283.0       5.3
         284.0       1.2
         285.0       1.1
         294.0       2.2
         295.0       6.8
         296.0       2.7
         297.0       4.7
         298.0       1.1
         308.0       2.1
         309.0       7.5
         310.0       3.0
         311.0       5.4
         312.0       1.3
         313.0       1.1
         322.0       1.2
         323.0       4.8
         324.0       1.9
         325.0       3.4
         330.0       1.7
         331.0       1.4
         336.0       1.0
         337.0       5.1
         338.0       1.9
         339.0       3.6
         351.0       5.9
         352.0       1.6
         353.0       4.2
         354.0       1.0
         366.0      27.7
         367.0       7.5
         368.0      19.4
         369.0       5.0
         370.0       4.0
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C19 H40 Cl2 Si 0.05 ml : 0.5 ml CDCl3
    dichloromethyloctadecylsilane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 1.493 B 1.36 C 1.26 D 1.109 E 0.879 F 0.761

         Hz     ppm     Int.
    

        591.67   1.481     22
        519.65   1.301     36
        502.69   1.258   1000
        489.75   1.226     35
        451.05   1.129     50
        445.68   1.116     21
        442.50   1.108     31
        434.69   1.088     42
        358.52   0.898     44
        351.81   0.881    137
        344.73   0.863     55
        304.20   0.762    367
    

in CDCl3



liquid film