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网站主页CAS数据库列表 10273-90-2更多图谱3-甲基-2-苯基吡啶(10273-90-2)质谱(MS)

3-甲基-2-苯基吡啶

产品名称 3-甲基-2-苯基吡啶

CAS号10273-90-2

分子式C12H11N

分子量169.22

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  • Mass

    MS-NW-9294          
    3-methyl-2-phenylpyridine
    C12H11N             (Mass of molecular ion:    169)
    

       Source Temperature: 240 °C
       Sample Temperature: 160 °C
       Reservoir, 75 eV
    

          39.0       6.3
          40.0       1.3
          50.0       1.4
          51.0       3.2
          63.0       3.1
          64.0       1.5
          65.0       3.0
          70.5       1.8
          71.5       1.5
          76.0       1.6
          77.0       3.9
          83.5      10.5
          84.0       2.7
          84.5       1.7
          89.0       1.4
         115.0       3.4
         139.0       2.5
         140.0       2.4
         141.0       3.0
         166.0       4.0
         167.0      24.8
         168.0     100.0
         169.0      30.0
         170.0       3.4
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C12 H11 N 0.05 ml : 0.5 ml CDCl3
    3-methyl-2-phenylpyridine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.509 B 7.51 C 7.418 D 7.359 E 7.119 F 2.310

         Hz     ppm     Int.
    

       3404.17   8.518    120
       3403.81   8.517    121
       3402.59   8.514    128
       3399.41   8.506    124
       3399.05   8.506    125
       3397.83   8.503    128
       3009.16   7.530    154
       3006.84   7.524    245
       3005.13   7.520    304
       3002.93   7.514    145
       3001.46   7.511    172
       2999.88   7.507    267
       2998.17   7.502    377
       2997.07   7.500    329
       2995.12   7.495     72
       2973.39   7.440    122
       2971.92   7.437    195
       2970.09   7.432     84
       2966.67   7.424    105
       2964.84   7.419    366
       2963.26   7.415    196
       2958.74   7.404    121
       2957.52   7.401    218
       2957.03   7.400    212
       2955.44   7.396     54
       2947.39   7.375    103
       2945.92   7.372    180
       2944.46   7.368    106
       2941.16   7.360     68
       2938.84   7.354    183
       2936.04   7.347     46
       2932.74   7.339     42
       2931.40   7.335     63
       2930.18   7.332     34
       2851.07   7.134    163
       2846.31   7.123    160
       2843.38   7.115    149
       2838.62   7.103    147
        923.46   2.311   1000
    

in CDCl3



liquid film