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网站主页CAS数据库列表 10477-94-8更多图谱3-甲基-5-苯基吡啶(10477-94-8)核磁图(1HNMR)

3-甲基-5-苯基吡啶

产品名称 3-甲基-5-苯基吡啶

CAS号10477-94-8

分子式C12H11N

分子量169.22

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  • Mass

    MS-IW-4779          
    3-methyl-5-phenylpyridine
    C12H11N             (Mass of molecular ion:    169)
    

       Source Temperature: 210 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          39.0       2.5
          50.0       1.4
          51.0       2.6
          52.0       1.0
          57.5       1.9
          63.0       2.8
          65.0       1.3
          69.5       1.3
          70.0       1.9
          70.5       1.6
          71.0       4.3
          74.0       1.2
          75.0       1.3
          76.0       2.3
          77.0       2.5
          83.5       1.4
          84.5       2.2
          89.0       1.6
          91.0       1.3
         102.0       4.6
         115.0       9.2
         116.0       1.8
         126.0       1.1
         127.0       2.7
         128.0       1.9
         139.0       3.2
         140.0       1.6
         141.0      12.5
         142.0       3.7
         143.0       1.0
         153.0       1.5
         154.0       5.4
         166.0       1.7
         167.0      11.4
         168.0      31.4
         169.0     100.0
         170.0      13.3
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C12 H11 N 0.05 ml : 0.5 ml CDCl3
    3-methyl-5-phenylpyridine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.634 B 8.390 C 7.597 D 7.508 E 7.406 F 7.341 G 2.324

         Hz     ppm     Int.
    

       3451.42   8.637    234
       3449.58   8.632    233
       3354.49   8.394    213
       3353.88   8.393    228
       3352.42   8.389    226
       3351.81   8.387    215
       3038.94   7.605    143
       3038.21   7.603    159
       3036.74   7.599    241
       3036.01   7.597    238
       3034.67   7.594    149
       3033.94   7.592    131
       3007.20   7.525    254
       3005.74   7.521    346
       3003.66   7.516    108
       2999.76   7.506    204
       2998.78   7.504    388
       2997.56   7.501    351
       2995.36   7.495     72
       2969.24   7.430    144
       2968.14   7.427    227
       2966.31   7.423     87
       2960.94   7.409    420
       2959.47   7.406    220
       2954.83   7.394    134
       2953.37   7.390    236
       2951.17   7.385     56
       2940.80   7.359    112
       2939.33   7.355    199
       2937.99   7.352    116
       2934.33   7.343     80
       2932.01   7.337    208
       2929.69   7.331     59
       2926.15   7.322     51
       2924.80   7.319     81
       2923.46   7.316     46
        929.08   2.325   1000
        928.34   2.323    941
    

in CDCl3



liquid film