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MS-NW-9294 3-methyl-2-phenylpyridine C12H11N (Mass of molecular ion: 169)
Source Temperature: 240 °C Sample Temperature: 160 °C Reservoir, 75 eV
39.0 6.3 40.0 1.3 50.0 1.4 51.0 3.2 63.0 3.1 64.0 1.5 65.0 3.0 70.5 1.8 71.5 1.5 76.0 1.6 77.0 3.9 83.5 10.5 84.0 2.7 84.5 1.7 89.0 1.4 115.0 3.4 139.0 2.5 140.0 2.4 141.0 3.0 166.0 4.0 167.0 24.8 168.0 100.0 169.0 30.0 170.0 3.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C12 H11 N 0.05 ml : 0.5 ml CDCl3 3-methyl-2-phenylpyridine Assign. Shift(ppm)
A 8.509 B 7.51 C 7.418 D 7.359 E 7.119 F 2.310
Hz ppm Int.
3404.17 8.518 120 3403.81 8.517 121 3402.59 8.514 128 3399.41 8.506 124 3399.05 8.506 125 3397.83 8.503 128 3009.16 7.530 154 3006.84 7.524 245 3005.13 7.520 304 3002.93 7.514 145 3001.46 7.511 172 2999.88 7.507 267 2998.17 7.502 377 2997.07 7.500 329 2995.12 7.495 72 2973.39 7.440 122 2971.92 7.437 195 2970.09 7.432 84 2966.67 7.424 105 2964.84 7.419 366 2963.26 7.415 196 2958.74 7.404 121 2957.52 7.401 218 2957.03 7.400 212 2955.44 7.396 54 2947.39 7.375 103 2945.92 7.372 180 2944.46 7.368 106 2941.16 7.360 68 2938.84 7.354 183 2936.04 7.347 46 2932.74 7.339 42 2931.40 7.335 63 2930.18 7.332 34 2851.07 7.134 163 2846.31 7.123 160 2843.38 7.115 149 2838.62 7.103 147 923.46 2.311 1000
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