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MassMS-NW-8399 2-phenylpyridine C11H9N (Mass of molecular ion: 155)
Source Temperature: 260 °C Sample Temperature: 140 °C Reservoir, 75 eV
27.0 1.5 39.0 3.0 50.0 6.6 51.0 12.7 52.0 5.8 62.0 1.7 63.0 4.2 64.0 1.5 74.0 3.1 75.0 3.5 76.0 5.5 76.5 2.4 77.0 11.6 77.5 3.0 78.0 4.8 79.0 1.1 89.0 1.3 101.0 2.2 102.0 5.0 103.0 2.7 104.0 1.3 115.0 1.9 126.0 3.2 127.0 11.1 128.0 9.5 129.0 2.3 152.0 1.1 153.0 3.3 154.0 61.7 155.0 100.0 156.0 11.9
parameter in CDCl3
400 MHz in CDCl3
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1H NMR 300 MHz C11 H9 N 2.5 M in CCl4 2-phenylpyridine 
Parameter ppm Hz
D(A) 7.984 D(B) 7.335 D(C) 7.272 J(A,A') 1.95 J(A,B) 7.90 J(A,B') 0.62 J(A,C) 1.25 J(A',B) 0.62 J(A',B') 7.90 J(A',C) 1.25 J(B,B') 1.42 J(B,C) 7.41 J(B',C) 7.41 D(D) 8.564 D(E) 6.981 D(F) 7.465 D(G) 7.537 J(D,E) 4.80 J(D,F) 1.87 J(D,G) 0.99 J(E,F) 7.86 J(E,G) 0.72 J(F,G) 8.01 GUENTHER,H. & CASTELLANO,S. BER.BUNSENGES.PHYSIK.CHEM. 70, 913 (1966)
Hz ppm Int.2573.03 8.577 325 2572.00 8.573 374 2571.23 8.571 378 2570.20 8.567 344 2568.25 8.561 346 2567.23 8.557 380 2566.41 8.555 380 2565.42 8.551 338 2400.20 8.001 684 2398.64 7.995 960 2396.48 7.988 272 2393.41 7.978 458 2391.75 7.972 909 2390.44 7.968 761 2388.09 7.960 103 2266.80 7.556 221 2265.84 7.553 404 2264.91 7.550 252 2258.80 7.529 503 2257.84 7.526 841 2256.91 7.523 480 2247.61 7.492 396 2245.78 7.486 390 2239.92 7.466 487 2238.09 7.460 488 2231.97 7.440 218 2230.14 7.434 217 2209.81 7.366 237 2208.17 7.361 366 2206.38 7.355 169 2201.25 7.337 1000 2199.80 7.333 430 2195.27 7.318 393 2193.88 7.313 766 2193.17 7.311 581 2191.44 7.305 138 2188.84 7.296 302 2187.31 7.291 588 2185.83 7.286 325 2182.84 7.276 168 2180.30 7.268 487 2177.11 7.257 94 2174.41 7.248 85 2173.02 7.243 135 2171.66 7.239 68 2100.86 7.003 341 2099.95 7.000 339 2096.06 6.987 344 2095.17 6.984 346 2093.25 6.977 321 2092.31 6.974 312 2088.41 6.961 304 2087.52 6.958 300
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1H NMR 399.65 MHz C11 H9 N 0.05 ml : 0.5 ml CDCl3 2-phenylpyridine Assign. Shift(ppm)
A 8.662 B 7.980 C 7.655 D 7.64 E 7.436 F 7.379 G 7.142
Hz ppm Int.3465.58 8.672 226 3464.23 8.669 401 3462.89 8.665 238 3460.82 8.660 249 3459.59 8.657 320 3458.01 8.653 235 3193.85 7.992 566 3192.38 7.988 847 3190.31 7.983 213 3187.01 7.975 361 3185.42 7.971 750 3184.20 7.968 635 3182.01 7.962 97 3064.82 7.669 74 3063.72 7.667 89 3059.94 7.657 943 3058.47 7.653 1000 3056.76 7.649 521 3055.66 7.646 512 3054.32 7.643 514 3052.61 7.639 459 3046.39 7.623 79 3044.68 7.619 85 2981.93 7.462 223 2980.59 7.459 362 2979.00 7.455 146 2973.63 7.441 864 2972.17 7.437 451 2967.53 7.426 288 2966.06 7.422 587 2963.99 7.417 113 2955.57 7.396 229 2954.10 7.392 417 2952.76 7.389 238 2949.22 7.380 149 2946.90 7.374 433 2944.34 7.368 105 2940.92 7.359 90 2939.58 7.356 150 2938.35 7.353 75 2865.97 7.172 32 2860.96 7.159 256 2857.91 7.152 242 2856.20 7.147 304 2855.59 7.146 267 2853.27 7.140 265 2852.42 7.138 272 2850.46 7.133 219 2847.53 7.126 258
in CDCl3
liquid film
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