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网站主页CAS数据库列表 1008-89-5更多图谱2-苯基吡啶(1008-89-5)核磁图(1HNMR)

2-苯基吡啶

产品名称 2-苯基吡啶

CAS号1008-89-5

分子式C11H9N

分子量155.2

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  • Mass

    MS-NW-8399          
    2-phenylpyridine
    C11H9N              (Mass of molecular ion:    155)
    

       Source Temperature: 260 °C
       Sample Temperature: 140 °C
       Reservoir, 75 eV
    

          27.0       1.5
          39.0       3.0
          50.0       6.6
          51.0      12.7
          52.0       5.8
          62.0       1.7
          63.0       4.2
          64.0       1.5
          74.0       3.1
          75.0       3.5
          76.0       5.5
          76.5       2.4
          77.0      11.6
          77.5       3.0
          78.0       4.8
          79.0       1.1
          89.0       1.3
         101.0       2.2
         102.0       5.0
         103.0       2.7
         104.0       1.3
         115.0       1.9
         126.0       3.2
         127.0      11.1
         128.0       9.5
         129.0       2.3
         152.0       1.1
         153.0       3.3
         154.0      61.7
         155.0     100.0
         156.0      11.9
    

parameter in CDCl3

400 MHz in CDCl3


  • 1H NMR 300 MHz
    C11 H9 N 2.5 M in CCl4
    2-phenylpyridine
    ChemicalStructure
        Parameter     ppm  Hz
    D(A) 7.984 D(B) 7.335 D(C) 7.272 J(A,A') 1.95 J(A,B) 7.90 J(A,B') 0.62 J(A,C) 1.25 J(A',B) 0.62 J(A',B') 7.90 J(A',C) 1.25 J(B,B') 1.42 J(B,C) 7.41 J(B',C) 7.41 D(D) 8.564 D(E) 6.981 D(F) 7.465 D(G) 7.537 J(D,E) 4.80 J(D,F) 1.87 J(D,G) 0.99 J(E,F) 7.86 J(E,G) 0.72 J(F,G) 8.01 GUENTHER,H. & CASTELLANO,S. BER.BUNSENGES.PHYSIK.CHEM. 70, 913 (1966)

         Hz     ppm     Int.
    

       2573.03   8.577    325
       2572.00   8.573    374
       2571.23   8.571    378
       2570.20   8.567    344
       2568.25   8.561    346
       2567.23   8.557    380
       2566.41   8.555    380
       2565.42   8.551    338
       2400.20   8.001    684
       2398.64   7.995    960
       2396.48   7.988    272
       2393.41   7.978    458
       2391.75   7.972    909
       2390.44   7.968    761
       2388.09   7.960    103
       2266.80   7.556    221
       2265.84   7.553    404
       2264.91   7.550    252
       2258.80   7.529    503
       2257.84   7.526    841
       2256.91   7.523    480
       2247.61   7.492    396
       2245.78   7.486    390
       2239.92   7.466    487
       2238.09   7.460    488
       2231.97   7.440    218
       2230.14   7.434    217
       2209.81   7.366    237
       2208.17   7.361    366
       2206.38   7.355    169
       2201.25   7.337   1000
       2199.80   7.333    430
       2195.27   7.318    393
       2193.88   7.313    766
       2193.17   7.311    581
       2191.44   7.305    138
       2188.84   7.296    302
       2187.31   7.291    588
       2185.83   7.286    325
       2182.84   7.276    168
       2180.30   7.268    487
       2177.11   7.257     94
       2174.41   7.248     85
       2173.02   7.243    135
       2171.66   7.239     68
       2100.86   7.003    341
       2099.95   7.000    339
       2096.06   6.987    344
       2095.17   6.984    346
       2093.25   6.977    321
       2092.31   6.974    312
       2088.41   6.961    304
       2087.52   6.958    300
    


  • 1H NMR 399.65 MHz
    C11 H9 N 0.05 ml : 0.5 ml CDCl3
    2-phenylpyridine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.662 B 7.980 C 7.655 D 7.64 E 7.436 F 7.379 G 7.142

         Hz     ppm     Int.
    

       3465.58   8.672    226
       3464.23   8.669    401
       3462.89   8.665    238
       3460.82   8.660    249
       3459.59   8.657    320
       3458.01   8.653    235
       3193.85   7.992    566
       3192.38   7.988    847
       3190.31   7.983    213
       3187.01   7.975    361
       3185.42   7.971    750
       3184.20   7.968    635
       3182.01   7.962     97
       3064.82   7.669     74
       3063.72   7.667     89
       3059.94   7.657    943
       3058.47   7.653   1000
       3056.76   7.649    521
       3055.66   7.646    512
       3054.32   7.643    514
       3052.61   7.639    459
       3046.39   7.623     79
       3044.68   7.619     85
       2981.93   7.462    223
       2980.59   7.459    362
       2979.00   7.455    146
       2973.63   7.441    864
       2972.17   7.437    451
       2967.53   7.426    288
       2966.06   7.422    587
       2963.99   7.417    113
       2955.57   7.396    229
       2954.10   7.392    417
       2952.76   7.389    238
       2949.22   7.380    149
       2946.90   7.374    433
       2944.34   7.368    105
       2940.92   7.359     90
       2939.58   7.356    150
       2938.35   7.353     75
       2865.97   7.172     32
       2860.96   7.159    256
       2857.91   7.152    242
       2856.20   7.147    304
       2855.59   7.146    267
       2853.27   7.140    265
       2852.42   7.138    272
       2850.46   7.133    219
       2847.53   7.126    258
    

in CDCl3



liquid film