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58-15-1

Aminopyrine

Product Name Aminopyrine

CAS58-15-1

MFC13H17N3O

MW231.29

More

  • 58-15-1_ms
    Mass

    MS-NW-8084          
    4-dimethylamino-2,3-dimethyl-1-phenyl-3-pyrazolin-5-one
    C13H17N3O           (Mass of molecular ion:    231)
    

       Source Temperature: 180 °C
       Sample Temperature: 140 °C
       Direct, 75 eV
    

          15.0      10.4
          18.0       2.8
          27.0       1.8
          28.0       7.5
          29.0       2.9
          30.0       1.7
          39.0       2.4
          40.0       1.0
          41.0       2.2
          42.0       9.7
          43.0       2.4
          44.0       2.3
          51.0       3.1
          54.0       2.8
          55.0       4.8
          56.0     100.0
          57.0       5.3
          64.0       1.7
          66.0       1.3
          67.0       2.7
          68.0       4.7
          69.0       1.8
          70.0       5.7
          71.0       8.2
          77.0       8.3
          82.0       4.0
          83.0       3.7
          84.0       1.2
          91.0       2.0
          97.0      41.2
          98.0       3.1
         104.0       1.3
         105.0       1.0
         111.0      13.3
         112.0       8.8
         115.5       1.3
         119.0       1.1
         121.0       1.2
         123.0       5.2
         132.0       1.1
         137.0       1.0
         147.0       1.2
         216.0       2.1
         230.0       4.6
         231.0      34.4
         232.0       5.9
    

90 MHz in CDCl3

  • 58-15-1_1hnmr

    1H NMR 89.56 MHz
    C13 H17 N3 O 0.038 g : 0.5 ml CDCl3
    4-dimethylamino-2,3-dimethyl-1-phenyl-3-pyrazolin-5-one
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.41 B 7.39 C 7.22 D 2.933 E 2.784 F 2.190 A,B AND C WERE CONFIRMED BY LAOCN PROGRAM.

         Hz     ppm     Int.
    

        666.50   7.442    136
        665.44   7.431     65
        664.63   7.422     38
        664.06   7.415     24
        663.94   7.414     24
        661.94   7.392    326
        657.50   7.342     26
        653.44   7.297     38
        651.94   7.280     28
        650.25   7.261     25
        648.38   7.240     22
        644.81   7.200     24
        262.75   2.934    645
        249.44   2.786   1000
        196.19   2.191    611
    

KBr disc

nujol mull