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MassMS-NW-6422 chlorodimethylphenylsilane C8H11ClSi (Mass of molecular ion: 170)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
39.0 1.8 43.0 2.6 50.0 1.7 51.0 4.1 53.0 3.0 63.0 15.7 64.0 1.0 65.0 6.8 77.0 2.0 77.5 1.9 78.0 1.1 79.0 1.9 91.0 13.7 92.0 1.3 93.0 4.0 95.0 1.3 103.0 1.9 105.0 3.2 119.0 2.8 135.0 4.3 139.0 1.2 155.0 100.0 156.0 12.8 157.0 35.0 158.0 4.3 159.0 1.3 170.0 16.5 171.0 2.4 172.0 6.1 193.0 1.3 271.0 2.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H11 Cl Si 0.05 ml : 0.5 ml CDCl3 chlorodimethylphenylsilane 
Assign. Shift(ppm)
A 7.613 B 7.40 C 7.38 D 0.653 J(SI-29,D) = 7.2 HZ
Hz ppm Int.3047.24 7.625 105 3045.53 7.621 126 3044.07 7.617 53 3043.33 7.615 51 3041.87 7.612 49 3039.79 7.607 97 3037.72 7.601 133 2959.72 7.406 42 2958.74 7.404 52 2955.69 7.396 47 2954.96 7.394 92 2953.00 7.389 225 2951.78 7.386 97 2950.93 7.384 115 2949.10 7.380 49 2947.27 7.375 75 2946.53 7.373 78 2945.80 7.371 103 2945.31 7.370 111 2943.48 7.366 37 2940.06 7.357 43 265.01 0.664 92 261.23 0.654 1000 257.93 0.646 123
in CDCl3
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