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Chlorodimethylphenylsilane

Product Name Chlorodimethylphenylsilane

CAS768-33-2

MFC8H11ClSi

MW170.71

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  • Mass 

    MS-NW-6422          
chlorodimethylphenylsilane
C8H11ClSi           (Mass of molecular ion:    170)


       Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV


          39.0       1.8
      43.0       2.6
      50.0       1.7
      51.0       4.1
      53.0       3.0
      63.0      15.7
      64.0       1.0
      65.0       6.8
      77.0       2.0
      77.5       1.9
      78.0       1.1
      79.0       1.9
      91.0      13.7
      92.0       1.3
      93.0       4.0
      95.0       1.3
     103.0       1.9
     105.0       3.2
     119.0       2.8
     135.0       4.3
     139.0       1.2
     155.0     100.0
     156.0      12.8
     157.0      35.0
     158.0       4.3
     159.0       1.3
     170.0      16.5
     171.0       2.4
     172.0       6.1
     193.0       1.3
     271.0       2.0

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C8 H11 Cl Si 0.05 ml : 0.5 ml CDCl3
    chlorodimethylphenylsilane
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             7.613
      B             7.40
      C             7.38
      D             0.653
     
     J(SI-29,D) = 7.2 HZ
  

         Hz     ppm     Int.


       3047.24   7.625    105
   3045.53   7.621    126
   3044.07   7.617     53
   3043.33   7.615     51
   3041.87   7.612     49
   3039.79   7.607     97
   3037.72   7.601    133
   2959.72   7.406     42
   2958.74   7.404     52
   2955.69   7.396     47
   2954.96   7.394     92
   2953.00   7.389    225
   2951.78   7.386     97
   2950.93   7.384    115
   2949.10   7.380     49
   2947.27   7.375     75
   2946.53   7.373     78
   2945.80   7.371    103
   2945.31   7.370    111
   2943.48   7.366     37
   2940.06   7.357     43
    265.01   0.664     92
    261.23   0.654   1000
    257.93   0.646    123

in CDCl3







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