SpectrumDetail Supplier Related Products
WebSite > CAS DataBase List  > 52-86-8More Spectrum  >Haloperidol(52-86-8)IR2

Haloperidol

CAS52-86-8

MFC21H23ClFNO2

MW375.86

More


  • Mass

    MS-IW-9284          
    4-(4-(p-chlorophenyl)-4-hydroxypiperidino)-4'-fluorobutyrophenone
    C21H23ClFNO2        (Mass of molecular ion:    375)
    

       Source Temperature: 170 °C
       Sample Temperature: 180 °C
       Direct, 75 eV
    

          15.0       1.2
          18.0       2.4
          27.0       2.3
          28.0       5.7
          29.0       1.7
          30.0       5.7
          39.0       1.8
          41.0       8.4
          42.0      72.2
          43.0       7.2
          44.0       2.5
          48.5       1.6
          50.0       1.2
          51.0       1.8
          53.0       1.2
          54.0       2.3
          55.0       8.3
          56.0      22.2
          57.0       4.3
          58.0       2.3
          60.0       3.6
          62.5       1.4
          63.0       1.3
          68.0       4.0
          69.0       3.4
          70.0      11.7
          71.0       7.9
          75.0       4.6
          76.0       1.1
          77.0       2.2
          82.0       4.6
          83.0      18.5
          84.0      14.6
          85.0       1.1
          86.0       4.8
          94.0       1.2
          95.0      15.1
          96.0       3.4
          97.0       1.1
          98.0       7.7
         101.0       1.6
         102.0       1.5
         103.0       1.7
         109.0       2.1
         111.0       4.3
         112.0       5.5
         113.0       1.9
         115.0       2.4
         123.0      35.6
         124.0       3.0
         125.0       6.3
         126.0       1.1
         127.0       3.8
         128.0       2.5
         129.0       4.5
         130.0       3.0
         131.0       1.0
         133.0       1.9
         135.0       1.3
         137.0       4.7
         138.0       2.6
         139.0       8.1
         140.0       1.0
         141.0       2.7
         149.0       1.3
         151.0       1.4
         154.0       1.9
         163.0       1.3
         164.0       2.7
         165.0      16.1
         166.0       2.6
         167.0       2.3
         176.0       4.8
         177.0       1.9
         189.0       5.7
         190.0       2.5
         191.0       2.3
         192.0       9.7
         193.0       1.9
         194.0       4.2
         196.0       1.0
         206.0      27.9
         207.0       4.1
         208.0      10.0
         209.0       2.7
         210.0       3.0
         211.0       1.0
         218.0       1.2
         219.0       4.5
         220.0       2.8
         221.0       2.8
         222.0       2.3
         224.0     100.0
         225.0      13.7
         226.0      32.5
         227.0       4.5
         236.0       1.0
         237.0      81.4
         238.0      12.4
         239.0      26.8
         240.0       3.9
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C21 H23 Cl F N O2 0.040 g : 0.5 ml DMSO-d6
    4-(4-(p-chlorophenyl)-4-hydroxypiperidino)-4'-fluorobutyrophenone
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.085 B *1 7.37 C 7.36 D *1 7.34 E 4.85 F 2.982 G 2.582 J 2.360 K 2.34 L 1.851 M 1.674 N 1.476 J(F-19,A)=5.6HZ J(F-19,C)=9.0HZ

         Hz     ppm     Int.
    

       3239.01   8.105    287
       3236.82   8.100    114
       3233.40   8.091    321
       3229.98   8.083    341
       3226.56   8.074    122
       3224.49   8.069    311
       3221.56   8.061     44
       2955.57   7.396     68
       2953.98   7.392    275
       2952.76   7.389    415
       2950.56   7.383    148
       2947.27   7.375    205
       2944.95   7.369    991
       2943.85   7.367    838
       2939.45   7.356    218
       2937.50   7.351   1000
       2934.94   7.344    491
       2931.03   7.334    152
       2928.71   7.329    315
       2926.88   7.324     59
       1936.40   4.846    500
       1198.73   3.000    197
       1192.02   2.983    457
       1185.18   2.966    217
       1037.72   2.597    137
       1027.10   2.570    167
        950.44   2.379    172
        943.60   2.362    463
        936.77   2.344    235
        932.86   2.335    216
        925.42   2.316     39
        921.88   2.307    111
        920.29   2.303     97
        919.92   2.302     97
        753.17   1.885     45
        746.46   1.868    173
        739.75   1.851    254
        732.91   1.834    166
        726.07   1.817     48
        684.81   1.714     65
        680.54   1.703     77
        671.88   1.682    145
        667.97   1.672    147
        659.42   1.650     98
        655.27   1.640     82
        595.09   1.490    213
        583.01   1.459    166
    

in DMSO-d6



KBr disc



nujol mull