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tert-Butylchlorodiphenylsilane

CAS58479-61-1

MFC16H19ClSi

MW274.86

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  • Mass

    MS-NW-7372          
    tert-butylchlorodiphenylsilane
    C16H19ClSi          (Mass of molecular ion:    274)
    

       Source Temperature: 220 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          29.0       2.2
          39.0       1.6
          41.0       3.1
          51.0       3.1
          53.0       2.0
          57.0       2.2
          63.0      14.5
          65.0       5.5
          77.0       2.2
          79.0       1.0
          91.0       1.3
         103.0       1.3
         105.0       3.0
         129.0       1.3
         139.0       2.0
         140.0       4.2
         141.0       2.3
         142.0       1.7
         152.0       2.5
         153.0       1.1
         155.0       5.1
         165.0       1.0
         180.0       3.3
         181.0      11.9
         182.0       2.4
         199.0       1.3
         215.0       2.9
         217.0     100.0
         218.0      18.5
         219.0      36.9
         220.0       6.5
         221.0       1.7
         274.0       1.7
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C16 H19 Cl Si 0.05 ml : 0.5 ml CDCl3
    tert-butylchlorodiphenylsilane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.757 B 7.41 C 7.37 D 1.134

         Hz     ppm     Int.
    

       3104.98   7.770    138
       3103.52   7.766    160
       3101.93   7.762     71
       3099.24   7.755     55
       3097.17   7.750    157
       3095.46   7.746    148
       2961.67   7.411     80
       2958.74   7.404     34
       2956.42   7.398     73
       2954.71   7.394    121
       2952.88   7.389     86
       2951.42   7.386    127
       2950.93   7.384    143
       2949.46   7.381     75
       2945.07   7.370     91
       2943.73   7.366    150
       2941.65   7.361     39
       2937.13   7.350     57
       2935.06   7.345     41
        456.54   1.143    105
        453.37   1.135   1000
        449.58   1.125     64
    

in CDCl3



liquid film