D/L-NORVALINOL

Mass

MS-NW-7302          
DL-2-amino-1-pentanol
C5H13NO             (Mass of molecular ion:    103)

   Source Temperature: 200 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      15.0       2.0
      18.0       4.4
      27.0       5.1
      28.0       7.3
      29.0       5.7
      30.0      56.2
      31.0       3.7
      39.0       3.6
      41.0       5.0
      42.0      14.5
      43.0       5.6
      44.0       9.0
      55.0       7.4
      56.0       3.5
      57.0       2.4
      60.0      28.7
      70.0       1.1
      72.0     100.0
      73.0       5.1
      86.0       5.0

Assign. Shift(ppm) A *1 3.548 B *1 3.261 C 2.94 D 2.78 E 1.38 F 1.26 G 0.93 J(A,B)=-10.7HZ J(A,D)=3.9HZ J(B,D)=7.6HZ

     Hz     ppm     Int.

    326.81   3.650    102
    323.00   3.607    123
    316.25   3.532    220
    312.38   3.488    234
    300.69   3.358    229
    297.00   3.317     30
    296.50   3.311     31
    293.06   3.273    287
    290.06   3.239    112
    287.44   3.210     34
    286.94   3.204     35
    286.44   3.199     35
    285.88   3.193     34
    282.50   3.155    179
    263.00   2.937   1000
    120.75   1.349    395
     88.50   0.989    273
     82.88   0.926    572
     77.50   0.866    229