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MS-NW-6777 3-pyrroline C4H7N (Mass of molecular ion: 69)
Source Temperature: 200 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 2.3 18.0 4.2 26.0 1.8 27.0 4.1 28.0 29.4 29.0 1.4 30.0 3.8 33.5 2.1 34.0 1.3 37.0 3.4 38.0 6.1 39.0 22.5 40.0 8.6 41.0 45.9 42.0 14.1 43.0 38.1 44.0 1.5 52.0 1.0 54.0 1.4 66.0 1.1 67.0 16.0 68.0 100.0 69.0 45.8 70.0 16.5 71.0 11.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C4 H7 N 0.05 ml : 0.5 ml CDCl3 3-pyrroline Assign. Shift(ppm)
A 5.860 B 2.84 C 1.68
Hz ppm Int.
2342.04 5.861 1000 2337.77 5.850 125 1141.97 2.858 337 1140.99 2.855 318 1139.40 2.851 325 1135.25 2.841 564 1131.10 2.831 307 1129.39 2.826 304 1128.54 2.824 320 677.12 1.695 223 673.46 1.686 264 670.41 1.678 518 667.24 1.670 243
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