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109-96-6

3-Pyrroline

Product Name 3-Pyrroline

CAS109-96-6

MFC4H7N

MW69.11

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  • 109-96-6_ms
    Mass

    MS-NW-6777          
    3-pyrroline
    C4H7N               (Mass of molecular ion:     69)
    

       Source Temperature: 200 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          15.0       2.3
          18.0       4.2
          26.0       1.8
          27.0       4.1
          28.0      29.4
          29.0       1.4
          30.0       3.8
          33.5       2.1
          34.0       1.3
          37.0       3.4
          38.0       6.1
          39.0      22.5
          40.0       8.6
          41.0      45.9
          42.0      14.1
          43.0      38.1
          44.0       1.5
          52.0       1.0
          54.0       1.4
          66.0       1.1
          67.0      16.0
          68.0     100.0
          69.0      45.8
          70.0      16.5
          71.0      11.7
    

400 MHz in CDCl3

  • 109-96-6_1hnmr

    1H NMR 399.65 MHz
    C4 H7 N 0.05 ml : 0.5 ml CDCl3
    3-pyrroline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 5.860 B 2.84 C 1.68

         Hz     ppm     Int.
    

       2342.04   5.861   1000
       2337.77   5.850    125
       1141.97   2.858    337
       1140.99   2.855    318
       1139.40   2.851    325
       1135.25   2.841    564
       1131.10   2.831    307
       1129.39   2.826    304
       1128.54   2.824    320
        677.12   1.695    223
        673.46   1.686    264
        670.41   1.678    518
        667.24   1.670    243
    

in CDCl3

  • 109-96-6_13cnmr

liquid film (CONTAINS 25% PYRROLIDINE)

  • 109-96-6_ir1

  • 109-96-6_raman