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(R)-(-)-Benzyl glycidyl ether

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(R)-(-)-Benzyl glycidyl ether Basic information
(R)-(-)-Benzyl glycidyl ether Chemical Properties
  • Melting point:88-93°C
  • Boiling point:130 °C (0.1 mmHg)
  • alpha -5.4 º (c=5 in toluene)
  • Density 1.077 g/mL at 25 °C(lit.)
  • refractive index n20/D 1.517(lit.)
  • Flash point:>230 °F
  • storage temp. 2-8°C
  • form paste (yellow)
  • Specific Gravity1.077
  • optical activity[α]20/D 5.4°, c = 5 in toluene
  • Water Solubility Soluble in water.
  • BRN 3588399
  • CAS DataBase Reference14618-80-5(CAS DataBase Reference)
Safety Information
  • Hazard Codes Xi
  • Risk Statements 36/37/38
  • Safety Statements 26-36-37/39
  • RIDADR NA 1993 / PGIII
  • WGK Germany 3
  • RTECS TX2860020
  • HS Code 29109000
  • Toxicitymic-sat 660 nmol/plate MUREAV 298,197,1993
MSDS
(R)-(-)-Benzyl glycidyl ether Usage And Synthesis
  • Chemical PropertiesColorless to light yellow liqui
  • Synthesis Reference(s)Tetrahedron Letters, 21, p. 4807, 1980 DOI: 10.1016/0040-4039(80)80145-6
  • Safety ProfileMutation data reported. Whenheated to decomposition it emits acrid smoke andirritating vapors.
  • Purification MethodsThis ether in EtOAc is dried (Na2SO4), then purified by flash chromatography using pet ether/EtOAc (5:1) as eluent. The ether distils through a short path distillation apparatus (Kügelrohr) as a colourless liquid. Alternatively, dissolve it in CHCl3, wash it with H2O, dry (Na2SO4), evaporate and purify by silica gel chromatography. [Anisuzzamen & Owen J Chem Soc 1021 1967, Takano et al. Heterocycles 1 6 381 1981, Lipshutz et al. Org Synth 69 82 1990, Takano et al. Synthesis 539 1989, Honda et al. Chem Pharm Bull Jpn 39 1385 1991, Beilstein 12 IV 2277.]
(R)-(-)-Benzyl glycidyl ether Preparation Products And Raw materials
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