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4-Chlorothiophenol

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4-Chlorothiophenol Basic information
4-Chlorothiophenol Chemical Properties
  • Melting point:49-51 °C(lit.)
  • Boiling point:205-207 °C(lit.)
  • Density 1.1911
  • refractive index 1.5480
  • Flash point:>230 °F
  • storage temp. 2-8°C
  • solubility methanol: soluble
  • form Crystalline Solid
  • pkapK1:5.9 (25°C)
  • color White to almost white
  • Water Solubility insoluble
  • Sensitive Stench/Lachrymatory
  • BRN 605971
  • InChIKeyVZXOZSQDJJNBRC-UHFFFAOYSA-N
  • CAS DataBase Reference106-54-7(CAS DataBase Reference)
  • NIST Chemistry ReferenceBenzenethiol, 4-chloro-(106-54-7)
  • EPA Substance Registry SystemBenzenethiol, 4-chloro- (106-54-7)
Safety Information
  • Hazard Codes C
  • Risk Statements 22-34-36/37-20/21/22
  • Safety Statements 26-36/37/39-45-27
  • RIDADR UN 3261 8/PG 2
  • WGK Germany 3
  • RTECS DC1050000
  • 9-13-23
  • Hazard Note Corrosive/Lachrymatory/Stench
  • TSCA Yes
  • HazardClass 8
  • PackingGroup III
  • HS Code 29309090
MSDS
4-Chlorothiophenol Usage And Synthesis
  • Chemical Propertieswhite to almost white crystalline solid
  • UsesOil additives, agricultural chemicals, plasticizers, rubber chemical, dyes, wetting agents, and stabilizers.
  • Synthesis Reference(s)The Journal of Organic Chemistry, 27, p. 4455, 1962 DOI: 10.1021/jo01059a081
    Synthetic Communications, 18, p. 575, 1988 DOI: 10.1080/00397918808064014
  • HazardToxic by ingestion.
  • Purification MethodsRecrystallise the thiophenol from aqueous EtOH. The SMe ether has m 129o and the SEt ether has m 64o. [D'Sousa et al. J Org Chem 52 1720 1987, Beilstein 6 H 326, 6 I 149, 6 III 1034.]
4-Chlorothiophenol Preparation Products And Raw materials
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