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SOLASODINE

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SOLASODINE Basic information
SOLASODINE Chemical Properties
  • Melting point:200-202°
  • alpha D25 -98° (c = 0.14 in methanol); D -113° (CHCl3)
  • Boiling point:532.75°C (rough estimate)
  • Density 1.0159 (rough estimate)
  • refractive index 1.6400 (estimate)
  • storage temp. 2-8°C
  • solubility DMSO: soluble0.5mg/mL, clear (warmed)
  • pkapKb 6.30(at 25℃)
  • form powder
  • color white to beige
  • optical activity[α]/D -88 to -98°, c = 0.2 in methanol
  • InChIKeyKOZCINYDCJVLDW-GCGBSLFCSA-N
  • CAS DataBase Reference126-17-0(CAS DataBase Reference)
  • NIST Chemistry ReferenceSolasodine(126-17-0)
Safety Information
SOLASODINE Usage And Synthesis
  • Usesantineoplastic, antiinflammatory
  • UsesA potentially useful precursor.
  • UsesStarting material for steroidal drugs.
  • Safety ProfilePoison by intraperitoneal route. Moderately toxic by ingestion. Experimental teratogenic and reproductive effects. When heated to decomposition it emits toxic fumes of NOx.
  • Purification MethodsSolasodine crystallises (as monohydrate) from MeOH as lustrous plates (on heating, the plates change to needles as they melt and resolidify in needles), or aqueous 80% EtOH, and sublimes at high vacuum. After recrystallisation from H2O, m 198-199o, then from Me2CO/H2O, m 199-201o, it has [] D 22 -109.3o (c 0.581, CHCl3). On TLC with silica gel G (*C6H6/absolute EtOH, 8:2) it has RF 0.45. IR (KBr): max at 10.3, 10.4, 11.2, 11.5 (azaoxaspirane bands). [Schreiber & Rnsch Tetrahedron 20 1939 1964, Uhle J Org Chem 27 656 1962, Kessar et al. Tetrahedron 27 2153 1971, Beilstein 27 III/IV 2000.]
SOLASODINE(126-17-0)Related Product Information
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