Phenetole
- Product Name:Phenetole
- CAS:103-73-1
- MF:C8H10O
- MW:122.16
- EINECS:203-139-7
- Mol File:103-73-1.mol
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Phenetole Chemical Properties
- Melting point:−30 °C(lit.)
- Boiling point:169-170 °C(lit.)
- Density 0.966 g/mL at 25 °C(lit.)
- refractive index n
20/D 1.507(lit.)
- Flash point:135 °F
- storage temp. Store below +30°C.
- solubility alcohol: freely soluble(lit.)
- form Liquid
- color Clear colorless to very slightly yellow
- Relative polarity2.9
- Water Solubility PRACTICALLY INSOLUBLE
- Sensitive Light Sensitive
- Merck 14,7229
- BRN 636270
- InChIKeyDLRJIFUOBPOJNS-UHFFFAOYSA-N
- CAS DataBase Reference103-73-1(CAS DataBase Reference)
- NIST Chemistry ReferenceBenzene, ethoxy-(103-73-1)
- EPA Substance Registry SystemBenzene, ethoxy- (103-73-1)
- Hazard Codes F,C
- Risk Statements 10-34-11
- Safety Statements 24/25-45-36/37/39-26-16
- RIDADR UN 1993 3/PG 3
- WGK Germany 2
- RTECS SI7700000
- TSCA Yes
- HazardClass 3
- PackingGroup III
- HS Code 29093090
- Hazardous Substances Data103-73-1(Hazardous Substances Data)
- ToxicityMLD in rats (mg/kg): 3500-4000 s.c. (Binet)
- Language:EnglishProvider:SigmaAldrich
- Language:EnglishProvider:ACROS
- Language:EnglishProvider:ALFA
Phenetole Usage And Synthesis
- Chemical PropertiesCLEAR COLOURLESS TO VERY SLIGHTLY YELLOW LIQUID
- DefinitionChEBI: An aromatic ether in which the ether oxygen is bonded to an ethyl and a phenyl group.
- Synthesis Reference(s)The Journal of Organic Chemistry, 55, p. 358, 1990 DOI: 10.1021/jo00288a065
Tetrahedron Letters, 29, p. 5553, 1988 DOI: 10.1016/S0040-4039(00)80811-4 - Purification MethodsSmall quantities of phenol can be removed by shaking with NaOH, but this is not a very likely contaminant of commercial material. Fractional distillation from sodium, at low pressures, probably gives adequate purification. It can be dissolved in diethyl ether and washed with 10% NaOH (to remove phenols), then water. The ethereal solution is evaporated, and the phenetole is fractionally distilled under vacuum. [Beilstein 6 H 140, 6 I 80, 6 II 142, 6 III 545.]
Phenetole Preparation Products And Raw materials
- Phenol Anisole Phenyl salicylate 2-Ethoxyethanol Ethoxyquin Ethylbenzene Phenacetin DIETHOXYMETHANE 2-Ethoxybenzoyl chloride Diphenyl ether Phenylacetic acid Ethylparaben 4-Ethoxybenzaldehyde 2,2-Diethoxyacetophenone Phenetole, p-bromo- 2-Ethoxybenzoic acid 2,3-DIFLUOROETHOXYBENZENE Methylphenyldiethoxysilane
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