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Tetrabutylammonium perchlorate

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Tetrabutylammonium perchlorate Basic information
Tetrabutylammonium perchlorate Chemical Properties
  • Melting point:211-215 °C
  • Density 1.0387 (rough estimate)
  • refractive index 1.6800 (estimate)
  • solubility acetonitrile: 0.1 g/mL, clear, colorless
  • form Crystalline Powder
  • color White
  • Water Solubility Soluble in acetonitrile and ethanol. Very slightly soluble in water.
  • Sensitive Hygroscopic
  • BRN 3579274
  • Stability:Stable. Strong oxidizer - contact with combustible material may cause fire. Incompatible with strong reducing agents, combustible materials. Do not heat.
  • CAS DataBase Reference1923-70-2(CAS DataBase Reference)
  • EPA Substance Registry System1-Butanaminium, N,N,N-tributyl-, perchlorate (1923-70-2)
Safety Information
  • Hazard Codes O,Xi
  • Risk Statements 5-8-36/37/38
  • Safety Statements 17-26-36-36/37/39
  • RIDADR UN 1479 5.1/PG 2
  • WGK Germany 3
  • TSCA Yes
  • HazardClass 5.1
  • PackingGroup II
  • HS Code 29239000
MSDS
Tetrabutylammonium perchlorate Usage And Synthesis
  • Chemical Propertieswhite powder
  • Purification MethodsCrystallise the perchlorate from EtOH ethyl acetate, from n-hexane or diethyl ether/acetone mixture, ethyl acetate or hot CH2Cl2. Dry it in a vacuum at room temperature over P2O5 for 24hours. [Anson et al. J Am Chem Soc 106 4460 1984, Ohst & Kochi J Am Chem Soc 108 2877 1986, Collman et al. J Am Chem Soc 108 2916 1986, Blau & Espenson J Am Chem Soc 108 1962 1986, Gustowski et al. J Am Chem Soc 108 1986, Ikezawa & Kutal J Org Chem 52 3299 1987, Beilstein 4 IV 557.]
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