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Tetrabutylammonium tetrafluoroborate

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Tetrabutylammonium tetrafluoroborate Basic information
Tetrabutylammonium tetrafluoroborate Chemical Properties
Safety Information
  • Hazard Codes Xi,T,Xn
  • Risk Statements 36/37/38-41-37/38-22
  • Safety Statements 26-36-37/39-39
  • RIDADR UN 1759 8/PG III
  • WGK Germany 3
  • Hazard Note Irritant/Hygroscopic
  • TSCA Yes
  • HazardClass TOXIC, HYGROSCOPIC
  • PackingGroup III
  • HS Code 29239000
MSDS
Tetrabutylammonium tetrafluoroborate Usage And Synthesis
  • Chemical PropertiesWHITE FINE CRYSTALLINE POWDER
  • Purification MethodsRecrystallise it from H2O, aqueous EtOH or from EtOAc by cooling in Dry-ice. Also recrystallise it from ethyl acetate/pentane or dry acetonitrile. Dry it at 80o under vacuum. [Detty & Jones J Am Chem Soc 109 5666 1987, Hartley & Faulkner J Am Chem Soc 107 3436 1985.] The acetate has m 118±2o (from BuCl), the bromide has m 118o (from EtOAc) and the nitrate has m 120o (from *C6H6). [Witschonka & Kraus J Am Chem Soc 69 2472 1947, Wheeler & Sandstedt J Am Chem Soc 77 2024 1955, Beilstein 4 IV 558.]
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