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4-Nitrobenzyl alcohol

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4-Nitrobenzyl alcohol Basic information
4-Nitrobenzyl alcohol Chemical Properties
  • Melting point:92-94 °C(lit.)
  • Boiling point:185 °C12 mm Hg(lit.)
  • Density 1.3585 (rough estimate)
  • refractive index 1.5030 (estimate)
  • Flash point:180 °C
  • storage temp. Sealed in dry,Room Temperature
  • solubility 2g/l
  • form Crystalline Powder
  • pka13.61±0.10(Predicted)
  • color Yellow
  • Water Solubility Soluble in water (2 mg/ml at 20°C).
  • BRN 1424026
  • InChIKeyJKTYGPATCNUWKN-UHFFFAOYSA-N
  • CAS DataBase Reference619-73-8(CAS DataBase Reference)
  • NIST Chemistry Reference4-NO2-C6H4CH2OH(619-73-8)
  • EPA Substance Registry SystemBenzenemethanol, 4-nitro- (619-73-8)
Safety Information
MSDS
4-Nitrobenzyl alcohol Usage And Synthesis
  • Chemical Propertieswhite to light yellow crystal powde
  • Uses4-Nitrobenzenemethanol is a potential building block in the synthesis of various pharmaceuticals.
  • DefinitionChEBI: A member of the class of benzyl alcohols that is benzyl alcohol substituted at the para-position by a nitro group.
  • Synthesis Reference(s)Organic Syntheses, Coll. Vol. 3, p. 652, 1955
    The Journal of Organic Chemistry, 55, p. 2968, 1990 DOI: 10.1021/jo00296a078
    Tetrahedron Letters, 19, p. 4985, 1978
  • Purification MethodsCrystallise the alcohol from EtOH and sublime it in vacuo. Purity should be at least 99.5%. Sublimed samples should be stored in the dark over anhydrous CaSO4 (Drierite). If the IR contains OH bands, then the sample should be resublimed before use. [Mohammed & Kosower J Am Chem Soc 93 2709 1979, Beilstein 6 IV 2611.]
4-Nitrobenzyl alcohol Preparation Products And Raw materials
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