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N-(Hydroxymethyl)phthalimide

N-(Hydroxymethyl)phthalimide Structure
N-(Hydroxymethyl)phthalimide
  • CAS No.118-29-6
  • Chemical Name:N-(Hydroxymethyl)phthalimide
  • CBNumber:CB1392676
  • Molecular Formula:C9H7NO3
  • Formula Weight:177.16
  • MOL File:118-29-6.mol
N-(Hydroxymethyl)phthalimide Property
Safety
  • Safety Statements  :22-24/25
  • WGK Germany  :3
  • RTECS  :TI5270000
  • TSCA  :Yes
  • HS Code  :29251995
Hazard and Precautionary Statements (GHS)
  • Symbol(GHS)
  • Signal word
  • Hazard statements H315-H319-H335
  • Precautionary statements P261-P280a-P304+P340-P305+P351+P338-P405-P501a
N-(Hydroxymethyl)phthalimide Price More Price(8)
  • Brand: Sigma-Aldrich
  • Product number: 8.14422
  • Product name : N-(Hydroxymethyl)-phthalimide
  • Purity: for synthesis
  • Packaging: 100 g
  • Price: $46.8
  • Updated: 2021/03/22
  • Buy: Buy
  • Brand: Sigma-Aldrich
  • Product number: 8.14422
  • Product name : N-(Hydroxymethyl)-phthalimide for synthesis. CAS 118-29-6, molar mass 177.16 g/mol., for synthesis
  • Purity: 
  • Packaging: 8144220100
  • Price: $48.9
  • Updated: 2020/08/18
  • Buy: Buy
  • Brand: Sigma-Aldrich
  • Product number: H41803
  • Product name : N-(Hydroxymethyl)phthalimide
  • Purity: 97%
  • Packaging: 100g
  • Price: $114
  • Updated: 2021/03/22
  • Buy: Buy
  • Brand: TCI Chemical
  • Product number: H0648
  • Product name : N-Hydroxymethylphthalimide
  • Purity: >98.0%(HPLC)(N)
  • Packaging: 25g
  • Price: $30
  • Updated: 2021/03/22
  • Buy: Buy
  • Brand: TCI Chemical
  • Product number: H0648
  • Product name : N-Hydroxymethylphthalimide
  • Purity: >98.0%(HPLC)(N)
  • Packaging: 250g
  • Price: $113
  • Updated: 2021/03/22
  • Buy: Buy

N-(Hydroxymethyl)phthalimide Chemical Properties,Usage,Production

  • Chemical Properties white crystalline powder
  • Definition ChEBI: A primary alcohol comprising phthalimide carrying an N-hydroxymethyl substituent.
  • Preparation To a flask equipped with a mechanical stirrer and condenser is added 511 gm (3.47 moles) of phthalimide, 260 ml of 40% formalin (3.47 moles), and 1750 ml of water. The mixture is refluxed for about 5-10 min or until a clear solution results (if any insoluble material remains, it is first filtered). Then the mixture is cooled for several hours. The resulting product is filtered with suction, washed with cold water, and air-dried to afford 594 gm (96%), m.p. 137-141°C.
    NOTE: The product should not be oven-dried since it decomposes with the loss of formaldehyde. Recrystallization of the product from ethanol affords 94% recovery of the original material with the same melting point range.
    Preparation of N-Hydroxymethylphthalimide
  • Synthesis Reference(s) Journal of the American Chemical Society, 77, p. 1913, 1955 DOI: 10.1021/ja01612a068
N-(Hydroxymethyl)phthalimide Preparation Products And Raw materials
Raw materials
Preparation Products
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