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MS-IW-7585 diphenyliodonium nitrate C12H10INO3 (Mass of molecular ion: 343)
Source Temperature: 170 °C Sample Temperature: 190 °C Direct, 75 eV
27.0 1.0 28.0 2.5 30.0 1.8 38.0 1.1 39.0 2.6 44.0 2.1 50.0 7.1 51.0 14.2 52.0 1.2 63.0 1.3 64.0 1.2 65.0 3.5 74.0 2.8 75.0 2.0 76.0 2.8 77.0 58.9 78.0 4.7 93.0 2.2 94.0 2.2 102.0 2.9 108.0 1.2 109.0 1.4 123.0 3.9 127.0 1.5 139.0 10.5 204.0 100.0 205.0 6.5 280.0 1.6
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C12 H10 I N O3 0.040 g : 0.5 ml DMSO-d6 diphenyliodonium nitrate Assign. Shift(ppm)
A 8.270 B 7.656 C 7.529
Hz ppm Int.
3312.50 8.289 112 3310.18 8.283 728 3309.08 8.280 917 3303.71 8.267 259 3301.88 8.262 969 3300.66 8.259 875 3069.46 7.681 113 3068.36 7.678 220 3067.26 7.675 153 3062.62 7.664 159 3060.91 7.659 534 3059.33 7.656 233 3054.57 7.644 219 3053.47 7.641 386 3052.37 7.638 243 3018.55 7.553 118 3016.24 7.548 711 3014.89 7.544 323 3008.42 7.528 1000 3002.56 7.513 198 3000.98 7.510 524 2998.90 7.504 133
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