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MS-NW-5665 3,3-diphenylpropylamine C15H17N (Mass of molecular ion: 211)
Source Temperature: 280 °C Sample Temperature: 190 °C Reservoir, 75 eV
18.0 2.5 27.0 1.8 28.0 3.3 30.0 86.5 31.0 3.3 39.0 4.6 42.0 1.5 43.0 2.1 44.0 7.2 50.0 2.1 51.0 6.3 52.0 1.4 56.0 1.1 58.0 2.9 62.0 1.0 63.0 3.4 65.0 2.8 75.0 1.3 76.0 1.7 77.0 10.0 78.0 3.8 79.0 1.9 89.0 2.6 91.0 5.1 93.0 3.3 102.0 2.1 103.0 10.4 104.0 5.4 105.0 1.3 106.0 9.5 107.0 1.2 115.0 10.1 116.0 18.5 117.0 7.6 118.0 1.1 128.0 2.3 132.0 2.7 133.0 2.3 139.0 1.9 141.0 1.4 151.0 1.4 152.0 10.4 153.0 3.5 163.0 1.3 164.0 1.9 165.0 26.4 166.0 9.7 167.0 33.0 168.0 20.1 169.0 3.0 178.0 7.0 179.0 15.1 180.0 3.9 181.0 1.6 192.0 1.2 193.0 48.5 194.0 100.0 195.0 14.9 196.0 1.2 211.0 10.9 212.0 2.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C15 H17 N 0.04 ml : 0.5 ml CDCl3 3,3-diphenylpropylamine Assign. Shift(ppm)
A 7.28 to 7.19 B 4.010 C 2.634 D 2.189 E 1.13
Hz ppm Int.
652.50 7.286 72 651.56 7.276 74 650.63 7.265 126 647.81 7.234 1000 645.69 7.210 216 644.00 7.191 126 642.31 7.172 44 641.75 7.166 49 637.44 7.118 30 359.44 4.014 56 351.88 3.929 32 237.81 2.656 40 237.44 2.652 39 230.38 2.573 38 205.94 2.300 31 205.06 2.290 34 198.25 2.214 65 197.69 2.208 63 192.19 2.146 36 190.75 2.130 45 101.56 1.134 63
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