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MassMS-NW-7372 tert-butylchlorodiphenylsilane C16H19ClSi (Mass of molecular ion: 274)
Source Temperature: 220 °C Sample Temperature: 190 °C Reservoir, 75 eV
29.0 2.2 39.0 1.6 41.0 3.1 51.0 3.1 53.0 2.0 57.0 2.2 63.0 14.5 65.0 5.5 77.0 2.2 79.0 1.0 91.0 1.3 103.0 1.3 105.0 3.0 129.0 1.3 139.0 2.0 140.0 4.2 141.0 2.3 142.0 1.7 152.0 2.5 153.0 1.1 155.0 5.1 165.0 1.0 180.0 3.3 181.0 11.9 182.0 2.4 199.0 1.3 215.0 2.9 217.0 100.0 218.0 18.5 219.0 36.9 220.0 6.5 221.0 1.7 274.0 1.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C16 H19 Cl Si 0.05 ml : 0.5 ml CDCl3 tert-butylchlorodiphenylsilane 
Assign. Shift(ppm)
A 7.757 B 7.41 C 7.37 D 1.134
Hz ppm Int.3104.98 7.770 138 3103.52 7.766 160 3101.93 7.762 71 3099.24 7.755 55 3097.17 7.750 157 3095.46 7.746 148 2961.67 7.411 80 2958.74 7.404 34 2956.42 7.398 73 2954.71 7.394 121 2952.88 7.389 86 2951.42 7.386 127 2950.93 7.384 143 2949.46 7.381 75 2945.07 7.370 91 2943.73 7.366 150 2941.65 7.361 39 2937.13 7.350 57 2935.06 7.345 41 456.54 1.143 105 453.37 1.135 1000 449.58 1.125 64
in CDCl3
liquid film
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