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网站主页CAS数据库列表 534-85-0更多图谱邻氨基二苯胺(534-85-0)Raman光谱

邻氨基二苯胺

产品名称 邻氨基二苯胺

CAS号534-85-0

分子式C12H12N2

分子量184.24

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  • Mass

    MS-NW-6882          
    N-phenyl-o-phenylenediamine
    C12H12N2            (Mass of molecular ion:    184)
    

       Source Temperature: 120 °C
       Sample Temperature: 110 °C
       Direct, 75 eV
    

          27.0       1.6
          28.0       2.1
          38.0       1.0
          39.0       4.4
          50.0       1.9
          51.0       6.1
          52.0       3.7
          53.0       3.5
          54.0       1.1
          63.0       1.9
          64.0       1.5
          65.0       5.6
          66.0       2.6
          77.0       5.5
          78.0       2.7
          79.0       2.6
          80.0       9.1
          81.0       1.6
          83.5       2.6
          90.0       1.0
          91.0       7.0
          91.5       2.1
          92.0       5.7
          93.0       1.7
         105.0       1.1
         107.0       5.7
         117.0       1.5
         118.0       4.1
         119.0       1.8
         128.0       1.0
         154.0       1.2
         156.0       2.6
         157.0       1.5
         158.0       1.6
         166.0       3.2
         167.0       3.2
         168.0       2.7
         169.0      24.3
         170.0       3.2
         181.0       5.4
         182.0      11.3
         183.0      32.3
         184.0     100.0
         185.0      13.9
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C12 H12 N2 0.043 g : 0.5 ml CDCl3
    N-phenyl-o-phenylenediamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.186 B 7.095 C 7.000 D 6.804 E 6.77 F 6.74 G 6.711 J 5.15 K 3.70

         Hz     ppm     Int.
    

       2884.16   7.217     43
       2881.84   7.211    101
       2879.88   7.207    534
       2877.69   7.201    216
       2872.44   7.188    740
       2871.22   7.185    724
       2869.26   7.180    129
       2865.84   7.171    230
       2863.89   7.166    650
       2861.69   7.161     92
       2843.99   7.117     30
       2840.33   7.108    369
       2838.87   7.104    418
       2835.57   7.096     36
       2832.52   7.088    399
       2831.05   7.084    455
       2805.91   7.021    227
       2804.44   7.018    227
       2798.58   7.003    343
       2797.97   7.002    335
       2797.12   6.999    345
       2793.70   6.991     30
       2790.65   6.983    306
       2789.18   6.980    288
       2727.66   6.826    165
       2726.56   6.823    297
       2725.46   6.820    189
       2720.34   6.807    253
       2719.24   6.805    514
       2718.26   6.802    291
       2715.33   6.795     47
       2712.89   6.789    176
       2711.79   6.786    290
       2710.69   6.783    215
       2709.72   6.781    409
       2708.25   6.777    535
       2701.42   6.760    576
       2700.32   6.757    546
       2699.95   6.756    533
       2696.66   6.748     72
       2693.85   6.741    457
       2692.38   6.737    392
       2687.99   6.726    176
       2686.04   6.721    904
       2684.81   6.718   1000
       2682.86   6.714    260
       2679.32   6.705    252
       2678.34   6.702    404
       2677.37   6.700    764
       2676.27   6.697    647
       2673.95   6.691     95
       2056.76   5.147     73
       1480.22   3.704     79
    


  • 1H NMR 89.56 MHz
    C12 H12 N2 0.042 g : 0.5 ml CDCl3
    N-phenyl-o-phenylenediamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.19 B 7.09 C 6.99 D 6.83 to 6.69 E 6.70 F 4.18 400MHZ : HSP-41-750

         Hz     ppm     Int.
    

        651.94   7.280    195
        651.00   7.269    255
        650.50   7.264    145
        649.19   7.249    143
        645.44   7.207    152
        644.19   7.193    737
        642.50   7.174    415
        641.25   7.161    186
        640.25   7.149    220
        638.56   7.130    468
        638.06   7.125    407
        636.00   7.102    692
        635.44   7.096    538
        633.94   7.079    254
        632.38   7.061    291
        631.13   7.048    573
        630.63   7.042    477
        629.69   7.031    191
        627.00   7.001    241
        626.44   6.995    280
        625.94   6.990    303
        620.75   6.932    538
        619.00   6.912    369
        616.69   6.886    162
        615.44   6.872    298
        614.19   6.858    291
        609.69   6.808   1000
        608.94   6.800    978
        607.94   6.789    852
        606.13   6.768    347
        605.00   6.756    728
        603.69   6.741    964
        603.13   6.735    887
        602.00   6.722    455
        601.31   6.715    468
        600.81   6.709    593
        600.13   6.701    289
        598.31   6.681    236
        597.81   6.675    243
        597.31   6.670    244
        596.50   6.661    632
        595.75   6.652    510
        595.31   6.648    553
        593.88   6.632    166
        374.13   4.178    144
    

in CDCl3



KBr disc



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