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MassMS-NW-0400 phenothiazine C12H9NS (Mass of molecular ion: 199)
Source Temperature: 160 °C Sample Temperature: 110 °C Direct, 75 eV
39.0 1.6 45.0 1.8 50.0 1.2 51.0 1.4 63.0 1.8 69.0 2.5 77.0 2.0 77.5 1.0 86.5 1.5 98.5 1.8 99.5 7.5 100.0 1.2 127.0 1.9 128.0 1.3 139.0 2.4 140.0 2.1 154.0 5.3 155.0 1.6 166.0 10.5 167.0 27.7 168.0 3.7 171.0 2.0 196.0 1.1 197.0 2.1 198.0 12.4 199.0 100.0 200.0 14.7 201.0 5.3
400 MHz at 49.0C
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1H NMR 399.65 MHz C12 H9 N S 0.034 g : 0.5 ml CDCl3 at 50C phenothiazine 
Assign. Shift(ppm)
A 6.96 B 6.95 C 6.785 D 6.490 E 5.7
Hz ppm Int.2785.03 6.969 635 2777.59 6.951 1000 2770.39 6.933 342 2768.92 6.929 247 2711.43 6.785 101 2597.53 6.500 207 2589.72 6.480 197
in DMSO-d6
KBr disc
nujol mull
AIBN CATALYZED OXIDATION
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